本发明涉及纤维素的水解,具体地说是一种在离子液体中高效水解纤维素的方法;以可溶解纤维素的离子液体为溶剂,以≥1摩尔当量的水为反应物,以催化量至化学计量的无机酸为催化剂,纤维素在常压下于70 ℃~100℃反应2分钟~9小时;反应结束后,用冷水淬灭反应、用碱中和,即得纤维素水解液;对水解液中总还原糖和葡萄糖进行化学定量分析,结果表明还原糖产率最高可达73%,对应的葡萄糖产率达到53%。与传统水解方法相比,本发明无需预处理过程、反应条件温和、水解活性高、反应速度快、酸耗少、对反应器的抗腐蚀性要求不高 ...
赵宗保, 李昌志
core
[Effects and mechanisms of PIT on wound healing of full-thickness skin defects in diabetic mice]. [PDF]
Zong YG, Huang WQ, Zhang Z, Peng Y.
europepmc +1 more source
本发明公开了一种再生纤维素复合膜,由以下质量百分比60%~97.5%的纤维素和2.5%~40%的卤代高分子组成,具有高韧性、可生物降解、相容性好等特点。本发明还公开了一种再生纤维素复合膜的制备方法,包括:1)将纤维素加入到预处理有机溶剂中,在155~165℃处理0.5~1h,再经过压榨;2)将压榨得到的预处理后的纤维素加入到共溶有机溶剂体系中,搅拌直至产生凝胶,再静置12~30h,得到透明溶液;3)向透明溶液中加入卤代高分子,搅拌共混20~40min,得到混合溶液;4)将混合溶液经过成膜和成膜后处理 ...
冯建湘, 刘小青, 张效敏, 朱锦
core
[Research progress on sample pretreatment technology for the analysis of new pollutants in food using composite covalent organic framework materials]. [PDF]
Sun ZY, Yuan GN, Niu YY, Ma JP.
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[<i>In Vitro</i> Biosafety Evaluation of Biodegradable Fluorinated Polyurethane Micelles]. [PDF]
Wang C +6 more
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[Research progress of cementless prosthesis in total knee arthroplasty]. [PDF]
Tai W, Qi X, Wang B, Chai W.
europepmc +1 more source
[Mesothelial impairment induced by peritoneal dialysis and its potential protective strategies]. [PDF]
Ban Y, Mei Y, Chen B, Tang W, Kang H.
europepmc +1 more source
[Research progress of gelatin composites in promoting peripheral nerve regeneration]. [PDF]
Zhang S +6 more
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[Efficacy and safety of emergency administration of tranexamic acid in elderly patients with intertrochanteric femoral fractures]. [PDF]
Rui C +10 more
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[Study on electrospun film-covered tracheal stents with adaptive release of anti-inflammatory drugs driven by the piezoelectric effect]. [PDF]
Wang Z +6 more
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