一种高效液相色谱手性固定相,其特征在于:该手性固定相是以键合在介孔骨架中的(1R,2R)-环己二胺作为手性选择剂的,含(1R,2R)-环己二胺的有机- 无机杂化介孔材料。本发明制备过程简单;手性官能团(1R,2R)-环己二胺是以共价键的方式键合在材料的骨架中,手性基团的掺杂量高;材料具有高比表面积 (1000~500m2/g)和均匀可调的孔径(在2~10nm之间可调变)。通过简单地改变硅酯的量可以调控球形材料的粒径大小。通过热处理的方法可以调变材料的孔径大小,在进行热处理调孔的过程中 ...
朱桂茹, 杨启华, 李 灿
core
Progress on functions of intracellular domain of trimeric ligand-gated ion channels. [PDF]
Lu Y, Lin Y, Wang J.
europepmc +1 more source
[Chinese consensus on autologous stem cell transplantation for adult acute leukemia (2024)]. [PDF]
Stem Cell Application Group +2 more
europepmc +1 more source
[A correction method for calculating resistance of Westerhof 's resistor]. [PDF]
Yang Y, Zou Y.
europepmc +1 more source
雷击是引发输电线路跳闸故障的主要原因之一,严重影响电网安全稳定运行。为有针对性地指导输电线路的防雷设计和改造,文中提出了基于多因素驱动的输电线路区域雷击跳闸风险评估方法。首先,综合考虑气象、电网、环境影响因素,构建完整有效的样本空间;其次,基于6种较优回归算法(XGBoost、RF、Bagging、GBRT、DT及KNN),对样本数据进行训练及验证;然后,选取拟合优度最高的XGBoost算法构建输电线路区域雷击跳闸风险评估模型;最后,算例结果表明:雷击故障点落在风险区域占75 ...
范凯 +4 more
doaj
[Prognostic analysis of plantar fasciitis treated by pneumatic ballistic extracorporeal shock wave versus ultrasound guided intervention]. [PDF]
Huo XL +7 more
europepmc +1 more source
[Chinese expert consensus on the diagnosis and treatment of acute graft-versus-host disease after hematopoietic stem cell transplantation (2024)]. [PDF]
Hematopoietic Stem Cell Application Group +2 more
europepmc +1 more source
[Clinical features and prognosis of 93 elderly patients with multiple myeloma]. [PDF]
Chen HM +5 more
europepmc +1 more source
[Rebound depolarization of substantia gelatinosa neurons and its modulatory mechanisms in rat spinal dorsal horn]. [PDF]
Li LC +5 more
europepmc +1 more source
[Changes in pain threshold and glial cell line-derived neurotrophic factor in rat model of trigeminal neuralgia]. [PDF]
Sijia Q +4 more
europepmc +1 more source

