Results 81 to 90 of about 1,328,781 (341)

Amphoteric Cu‐Doping Leading to High Thermoelectric Performance in p‐Type Bismuth Antimony Telluride

open access: yesAdvanced Functional Materials, EarlyView.
This study shows that Cu plays two opposite roles in p‐type Bi0.5Sb1.5Te3 depending on the processing route. Under thermodynamic‐equilibrium bulk‐synthesis, Cu mainly occupies cation sites, increases hole concentration, preserves mobility, and slightly reduces lattice heat transport. The best‐performing composition among the investigated series reaches
Moritz Thiem   +15 more
wiley   +1 more source

Listening to the Formation of Polymorphs in a Ball Mill

open access: yesAnalytical Chemistry
IIn this contribution, we apply our newly developed ball-milling operando platform, which combines Raman spectroscopy, thermal (IR) imaging, as well as acoustic and high-speed optical video recordings, to the synthesis and transformation of citric acid – isonicotinamide (1 : 2) cocrystal polymorphs in transparent PMMA jars. Particularly, we demonstrate
Eloïse Marie Samantha Parlier   +5 more
openaire   +3 more sources

Nitride MXenes Beyond Carbides: Bridging the Gap Between Computational Prediction and Experimental Realization

open access: yesAdvanced Functional Materials, EarlyView.
Nitride MXenes remain constrained by a persistent gap between computational prediction and experimental realization. This Review identifies the thermodynamic, kinetic, and chemical barriers limiting their synthesis, critically evaluates emerging fabrication routes, and proposes a multidimensional computational‐experimental framework to accelerate the ...
Naresh Varnakavi, Masoud Soroush
wiley   +1 more source

Redox reactions of small organic molecules using ball milling and piezoelectric materials

open access: yesScience, 2019
Redox catalysis in a ball mill Mixing solid reactants in a ball mill is a promising means of avoiding the copious solvent waste associated with most chemical syntheses. Kubota et al.
Koji Kubota   +3 more
semanticscholar   +1 more source

Unified Pressure and Field Response Across Distinct Charge‐Order Regimes in Ti‐Doped CsV3Sb5

open access: yesAdvanced Functional Materials, EarlyView.
We microscopically investigate the interplay between charge order and superconductivity in a kagome superconductor across regimes of long‐ and short‐range charge order. Hydrostatic‐pressure and magnetic‐field μSR$\mu{\rm SR}$ measurements reveal remarkably similar superconducting and normal‐state time‐reversal‐symmetry‐breaking responses in both ...
P. Kral   +12 more
wiley   +1 more source

Beyond Presumptions: Toward Mechanistic Clarity in Metal‐Free Carbon Catalysts for Electrochemical H2O2 Production via Data Science

open access: yesAdvanced Materials, EarlyView.
Metal‐free carbon catalysts enable the sustainable synthesis of hydrogen peroxide via two‐electron oxygen reduction; however, active site complexity continues to hinder reliable interpretation. This review critiques correlation‐based approaches and highlights the importance of orthogonal experimental designs, standardized catalyst passports ...
Dayu Zhu   +3 more
wiley   +1 more source

Surface Functionalization of Anatase Nanopowders with Stearic Acid by Ball Milling

open access: yesMolecules
This contribution is focused on the functionalization of the surface of anatase nanopowders following their mechanical processing by ball milling in the presence of stearic acid.
Maria Carta   +4 more
doaj   +1 more source

Sustainable Approaches to Nanomaterial synthesis Using Mechanical Grinding Methods [PDF]

open access: yesInternational Journal of Industry and Sustainable Development
This study provides a comprehensive examination of the Mechanical Grinding (MG) technique, with a particular emphasis on ball milling as a prominent top-down method for the synthesis of nanomaterials.
Mohamed Bassyouni   +2 more
doaj   +1 more source

Wet ball milling of zeolite HY

open access: yesPowder Technology, 2004
Abstract Wet ball milling, as a potential means to decrease the particle size of zeolite HY with minimal loss of crystallinity, was investigated. The diameter of the ball as well as the milling speed and time were varied in the experiments. Particle size distributions of the commercial zeolite HY and the ground samples were obtained to determine the ...
Akcay, K   +4 more
openaire   +2 more sources

Pulsed Laser‐Assisted Phase Engineering of Multimetallic Colloidal Nanocrystals With Complex Compositions

open access: yesAdvanced Materials, EarlyView.
The engineering of colloidal nanocrystals with complex compositions has emerged as a highly active area of research within nanomaterials science. This review covers key aspects of colloidal solid‐solution nanocrystal formation using pulsed laser irradiation.
Marina T. Candela   +4 more
wiley   +1 more source

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