Results 251 to 260 of about 458,942 (313)

High-pressure liquid chromatography of steroids

Journal of Chromatography A, 1979
After a brief discussion of the merits and limitations of high-pressure liquid chromatography (HPLC) relative to other chromatographic methods, special problems in the application to steroids are discussed. Publications on HPLC of steroids are then discussed under the headings of individual classes, arranged generally in the order of increasing ...
E, Heftmann, I R, Hunter
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High-pressure liquid chromatography of peptides

Journal of Chromatography A, 1977
Peptides varying in size from di- to decapeptide have been subjected to high-pressure liquid chromatography on Phenyl-Corasil, Poragel PN, and Poragel PS under reversed-phase conditions with acetonitrile-water mixtures. It has been found that residual silanol groups in the Phenyl-Corasil and the functional groups in the Poragels significantly influence
J J, Hansen, T, Greibrokk, B L, Currie, K N, Johansson, K, Folkers   +4 more
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High-back-pressure liquid chromatography

Journal of Chromatography A, 1982
Abstract The retention behaviour of solutes on various stationary phases was studied by micro-high-performance liquid chromatography using liquefied solvents as the mobile phase. An octadecylsilylated stationary phase discriminates between coplanar and non-planar aromatic hydrocarbons in the normal-phase system using isobutane as the mobile phase ...
Toyohide Takeuchi, Daido Ishii
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Laboratory Automation of High‐Pressure Liquid Chromatography

Journal of Pharmaceutical Sciences, 1975
An automated system for high-pressure liquid chromatography was developed. The system is built around commercial modules wherever possible, modified to varying degrees. An automatic sampler, a sample pump, a high-pressure sampling valve, a recorder with an integrator, and a high-pressure liquid chromatograph comprise the commercial instruments. Relays,
W F, Beyer, D D, Gleason
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Thimerosal Determination by High-Pressure Liquid Chromatography

Journal of Pharmaceutical Sciences, 1978
A sensitive and useful high-pressure liquid chromatographic method for the determination of intact thimerosal was developed. This method is extremely fast and reliable, and its inherent specificity makes it a breakthrough over other common wet chemical methods.
R C, Meyer, L B, Cohn
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Effects of high pressure in liquid chromatography

Journal of Chromatography A, 2005
All the experimental parameters that the chromatographers are used to consider as constant (the column length and its diameter, the particle size, the column porosities, the phase ratio, the column hold-up volume, the pressure gradient along the column, the mobile phase density and its viscosity, the diffusion coefficients, the equilibrium constants ...
Martin, Michel, Guiochon, Georges
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High pressure liquid chromatography of neutral glycosphingolipids

Biochimica et Biophysica Acta (BBA) - Lipids and Lipid Metabolism, 1972
Abstract A system for the separation of neutral glycosphingolipids by high pressure liquid chromatography of their benzoylated derivatives has been devised. Serum mono-, di-, tri-and tetraglycosylceramides are completely resolved within 25 min. A full scale recorder response can be obtained with approximately 1.0 nmole of glycolipid.
J E, Evans, R H, McCluer
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Anthracycline Assay by High-pressure Liquid Chromatography

Journal of Pharmaceutical Sciences, 1981
A general method of analysis of anthracycline concentrations was developed. Drug is extracted from plasma with organic solvent and separated from metabolites by high-pressure liquid chromatography on an aminocyanosilica column. Detection and quantitation are by the endogenous fluorescence of compounds having an intact tetracyclic ring structure. Limits
S D, Averbuch, T T, Finkelstein, S E, Fandrich, S D, Reich   +3 more
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High-pressure liquid chromatography of steroidal alkaloids

Journal of Chromatography A, 1976
High-pressure liquid chromatography was used to separate the following steroidal alkaloids: tomatidine, solanidine, solasodine, rubijervine, veratramine and jervine. The method was used to prepare crystalline solanidine from a crude mixture of aglycones obtained from Solanum chacoense, and to separate radioactive solanidine from extracts of potato ...
I R, Hunter, M K, Walden, J R, Wagner, E, Heftmann   +3 more
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Method transfer from high-pressure liquid chromatography to ultra-high-pressure liquid chromatography. I. A thermodynamic perspective

Journal of Chromatography A, 2014
This is the first investigation in a series that aims to enhance the scientific knowledge needed for reliable analytical method transfer between HPLC and UHPLC using the quality by design (QbD) framework. Here, we investigated the differences and similarities from a thermodynamic point of view between RP-LC separations conducted with 3.5μm (HPLC) and 1.
Dennis, Åsberg, Marek, Leśko, Jörgen, Samuelsson, Krzysztof, Kaczmarski, Torgny, Fornstedt   +4 more
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