A method validation for simultaneous determination of phthalates and bisphenol A released from plastic water containers [PDF]
Phthalates (or phthalate esters, PAEs) and bisphenol A (BPA) are widely used in various industries, particularly in the fields of cosmetics and packaging, and they increase the malleability and workability of materials.
Avino, P. +4 more
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Kinetic Resolution in Asymmetric Epoxidation using Iminium Salt Catalysis [PDF]
The first reported examples of kinetic resolution in epoxidation reactions using iminium salt catalysis are described, providing up to 99% ee in the epoxidation of racemic cis ...
Allin, Steven M. +7 more
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A highly efficient technique has been developed for the resolution of several sterols that are intermediates in the biosynthesis of cholesterol and that differ only by one carbon-carbon double bond or by one methyl group. The technique described utilizes
E Hansbury, T J Scallen
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Characterization and toxicity evaluation of degradation products of febantel
Background The aim of the present work was to determine potential toxicity of degradation products of febantel generated under different stress conditions mentioned in guideline Q1A (R2) laid down by International Council for Harmonization (ICH).
Anand A. Mahajan +4 more
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Effects of ultrasonic waves on enhancement of relative volatilities in methanol-water mixtures [PDF]
The application of ultrasonic wave in various fields including separation process has increased predominantly. This paper reports the practicability of using ultrasonic wave to enhance separation of binary mixtures by distillation.
Abdul Mudalip, Siti Kholijah +2 more
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Purpose. The purpose of this research is to develop new, highly sensitive and selective method for determination of piperidinium 2-((5-(furan-2-yl)-4-phenyl-4H-1,2,4-triazol-3-yl)thio)acetate as an active pharmaceutical ingredient (API) in 1 % injection ...
B. O. Varynskyi +2 more
doaj +1 more source
Purpose. A development and validation of new sensitive, high efficient and selective HPLC determination method of intermediates technological contaminations in bulk drug of morpholin-4-ium 2-((4-(2-methoxyphenyl)-5-(pyridine-4-yl)-4H-1,2,4-triazole-3-yl ...
B. O. Varynskyi, A. G. Kaplaushenko
doaj +1 more source
Analysis of free analyte fractions by rapid affinity chromatography [PDF]
The invention is generally directed toward an analytical method to determine the concentration of the free analyte fraction in a sample. More particularly, the method encompasses applying a sample comprising a free and bound analyte fraction to an ...
Clarke, William A., Hage, David S.
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ABSORPTION OF CONTROLLED RELEASE MORPHINE SULPHATE IN THE IMMEDIATE POSTOPERATIVE PERIOD [PDF]
The absorption of morphine sulphate, given orally as a controlled release preparation, was studied in 10 patients who had undergone peripheral vascular surgery with a standard opioid-based general anaesthetic technique. Serum morphine concentrations were
ACHOLA, K. J. +3 more
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Multi-residue analysis of pharmaceuticals in Belgian surface water : a novel screening-to-quantification approach using large-volume injection liquid chromatography coupled to high-resolution mass spectrometry [PDF]
The ever growing number of emerging micropollutants such as pharmaceuticals requests rapid and sensitive full-spectrum analytical techniques. Time-of-flight highresolution mass spectrometry (TOF-HRMS) is a promising alternative for the state-ofthe- art ...
Demeestere, Kristof +3 more
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