Results 81 to 90 of about 756,054 (237)

A method validation for simultaneous determination of phthalates and bisphenol A released from plastic water containers [PDF]

open access: yes, 2019
Phthalates (or phthalate esters, PAEs) and bisphenol A (BPA) are widely used in various industries, particularly in the fields of cosmetics and packaging, and they increase the malleability and workability of materials.
Avino, P.   +4 more
core   +1 more source

Kinetic Resolution in Asymmetric Epoxidation using Iminium Salt Catalysis [PDF]

open access: yes, 2013
The first reported examples of kinetic resolution in epoxidation reactions using iminium salt catalysis are described, providing up to 99% ee in the epoxidation of racemic cis ...
Allin, Steven M.   +7 more
core   +1 more source

Resolution of desmosterol, cholesterol, and other sterol intermediates by reverse-phase high-pressure liquid chromatography.

open access: yesJournal of Lipid Research, 1978
A highly efficient technique has been developed for the resolution of several sterols that are intermediates in the biosynthesis of cholesterol and that differ only by one carbon-carbon double bond or by one methyl group. The technique described utilizes
E Hansbury, T J Scallen
doaj   +1 more source

Characterization and toxicity evaluation of degradation products of febantel

open access: yesFuture Journal of Pharmaceutical Sciences, 2020
Background The aim of the present work was to determine potential toxicity of degradation products of febantel generated under different stress conditions mentioned in guideline Q1A (R2) laid down by International Council for Harmonization (ICH).
Anand A. Mahajan   +4 more
doaj   +1 more source

Effects of ultrasonic waves on enhancement of relative volatilities in methanol-water mixtures [PDF]

open access: yes, 2008
The application of ultrasonic wave in various fields including separation process has increased predominantly. This paper reports the practicability of using ultrasonic wave to enhance separation of binary mixtures by distillation.
Abdul Mudalip, Siti Kholijah   +2 more
core   +1 more source

Development and validation of HPLC-DAD method of determination piperidinium 2-((5-(furan-2-yl)-4-phenyl-4H-1,2,4-triazol-3-yl)thio)acetate in 1 % solution

open access: yesZaporožskij Medicinskij Žurnal, 2017
Purpose. The purpose of this research is to develop new, highly sensitive and selective method for determination of piperidinium 2-((5-(furan-2-yl)-4-phenyl-4H-1,2,4-triazol-3-yl)thio)acetate as an active pharmaceutical ingredient (API) in 1 % injection ...
B. O. Varynskyi   +2 more
doaj   +1 more source

The development and validation of HPLC-DMD method for intermediate products impurities determination of morpholinium 2-((4-(2-methoxyphenyl)-5-(pyridine-4-yl)-4H-1,2,4-triazole-3-yl)thio)acetate in bulk drug

open access: yesZaporožskij Medicinskij Žurnal, 2017
Purpose. A development and validation of new sensitive, high efficient and selective HPLC determination method of intermediates technological contaminations in bulk drug of morpholin-4-ium 2-((4-(2-methoxyphenyl)-5-(pyridine-4-yl)-4H-1,2,4-triazole-3-yl ...
B. O. Varynskyi, A. G. Kaplaushenko
doaj   +1 more source

Analysis of free analyte fractions by rapid affinity chromatography [PDF]

open access: yes, 2004
The invention is generally directed toward an analytical method to determine the concentration of the free analyte fraction in a sample. More particularly, the method encompasses applying a sample comprising a free and bound analyte fraction to an ...
Clarke, William A., Hage, David S.
core   +1 more source

ABSORPTION OF CONTROLLED RELEASE MORPHINE SULPHATE IN THE IMMEDIATE POSTOPERATIVE PERIOD [PDF]

open access: yes, 2017
The absorption of morphine sulphate, given orally as a controlled release preparation, was studied in 10 patients who had undergone peripheral vascular surgery with a standard opioid-based general anaesthetic technique. Serum morphine concentrations were
ACHOLA, K. J.   +3 more
core  

Multi-residue analysis of pharmaceuticals in Belgian surface water : a novel screening-to-quantification approach using large-volume injection liquid chromatography coupled to high-resolution mass spectrometry [PDF]

open access: yes, 2013
The ever growing number of emerging micropollutants such as pharmaceuticals requests rapid and sensitive full-spectrum analytical techniques. Time-of-flight highresolution mass spectrometry (TOF-HRMS) is a promising alternative for the state-ofthe- art ...
Demeestere, Kristof   +3 more
core  

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