Synthesis of Bulk Superconducting LiNbO2 Crystals Through CaH2 Reduction
Advanced Materials, EarlyView.CaH2 reduction reconstructively transforms insulating LiNbO3 single crystals into superconducting bulk LiNbO2 with a critical temperature of Tc = 14.4 K. Scanning electron microscopy reveals large‐volume, high‐yield phase conversion. Magnetization measurements demonstrate a robust ∼ 77% Meissner shielding fraction, establishing bulk superconductivity ...
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