Results 31 to 40 of about 2,120 (176)

Chemical Ionization Mass Spectrometry: Fundamental Principles, Diverse Applications, and the Latest Technological Frontiers

Mass Spectrometry Reviews, EarlyView.
ABSTRACT The review examines the evolution of chemical ionization mass spectrometry (CI‐MS), a technique developed in 1966 by Field and Munson. CI is a soft‐ionization method that produces more intense molecular ions with less fragmentation than electron ionization (EI).
Malvika Dutt, Adriana Arigò, Giorgio Famiglini, Pierangela Palma, Achille Cappiello   +4 more
wiley   +1 more source

Magnetic Ionic Liquids in Sample Preparation: Recent Advances and Future Trends

Separations, 2021
In the last decades, a myriad of materials has been synthesized and utilized for the development of sample preparation procedures. The use of their magnetic analogues has gained significant attention and many procedures have been developed using magnetic
Theodoros Chatzimitakos, Phoebe Anagnostou, Ioanna Constantinou, Kalliroi Dakidi, Constantine Stalikas   +4 more
doaj   +1 more source

Recent Advances (2023–2025) of Capillary Electrophoresis‐Mass Spectrometry (CE‐MS) for Top‐Down Proteomics

Mass Spectrometry Reviews, EarlyView.
ABSTRACT Top‐down proteomics (TDP) characterizes proteoforms in cells, tissues, and biofluids, in discovery mode and on a global scale, requiring analytical tools with high peak capacity for proteoform separation and high sensitivity for proteoform detection, given the extremely high proteoform complexity and wide proteoform concentration dynamic range.
Guijie Zhu, David A. Alvarez Rodriguez, Noah Gould, Alexander R. Ivanov, Kevin Jooß, Liangliang Sun   +5 more
wiley   +1 more source

Solidification floating organic drop for dispersive liquid–liquid microextraction estimation of copper in different water samples

Green Processing and Synthesis
A selective, sensitive, and eco-friendly microextraction method followed by the solidified floating organic drop-dispersive liquid–liquid microextraction was investigated to determine copper(ii) ions by spectrophotometry.
Fraihat Safwan Mohammad
doaj   +1 more source

Schiff Base‐UiO66 Composite‐based Dispersive Micro Solid‐Phase Extraction of Pesticides From Fruit Juices Combined With Dispersive Liquid‐Liquid Microextraction Prior to Gas Chromatography‐Flame Ionisation Detection

Analytical Science Advances, Volume 7, Issue 2, December 2026.
ABSTRACT A dispersive micro solid‐phase extraction method was introduced using a Schiff base‐UiO66 nanocomposite as the adsorbent in the extraction of multi‐class pesticide residues in pear, cherry, grape, and apricot juices. The extraction procedure was hyphenated with a liquid‐phase microextraction procedure, providing a high preconcentration factor ...
Behnam Hosseininezhad, Mahdi Bomorovat, Mahboob Nemati, Mir Ali Farajzadeh, Ramin Atazadeh, Mohammad Reza Afshar Mogaddam   +5 more
wiley   +1 more source

Optimized SPE‐HPLC‐FLD Method for the Simultaneous Determination of Olaparib, Propranolol, and Furosemide in Human Urine

Biomedical Chromatography, Volume 40, Issue 8, August 2026.
ABSTRACT Olaparib belongs to the PARP inhibitors and is widely used as an anticancer drug. Due to frequent side effects, it is usually co‐administered with an antihypertensive, such as propranolol and/or an antidiuretic, such as furosemide. In this study, a highly sensitive HPLC‐FLD method was developed for the simultaneous determination of the three ...
Georgios Kamaris, Antonia Kalagia, Catherine K. Markopoulou   +2 more
wiley   +1 more source

Valproic acid extraction methods in human samples for gas chromatography analysis: a review

Drug Analytical Research
Valproic acid (VPA) is widely used as an important drug for the treatment of epilepsy, seizures, bipolar disorders, and migraines. However, its narrow therapeutic range lead to risks of unintentional poisoning and potential suicide.
Juliana Blume de Oliveira, Bruno Pereira dos Santos, Marcelo Arbo   +2 more
doaj   +1 more source

Ion pair-dispersive liquid-liquid microextraction of trace amount of rhodium ion in water and road dust samples prior to flame atomic absorption spectrometry determination

Química Nova, 2011
A simple ion pair-dispersive liquid-liquid microextraction method was proposed for preconcentration trace amounts of rhodium. An ion association complex of RhCl4- and tetradecyldimetylbenzylamonium was extracted into cholorobenzene.
Daryoush Afzali, Ali Ghazizadeh, Hassan Salari   +2 more
doaj   +1 more source

Liquid-phase microextraction of polycyclic aromatic hydrocarbons: A review

Reviews in Analytical Chemistry, 2020
Polycyclic aromatic hydrocarbons (PAHs) are a large group of organic compounds comprised of two or more fused benzene rings, which arise from the incomplete combustion of organic materials. These compounds have been of concern as carcinogens and mutagens
Jalili Vahid, Barkhordari Abdullah, Ghiasvand Alireza   +2 more
doaj   +1 more source

Green and Rapid Determination of Phthalates in Mineral Water From Virgin and Recycled PET Bottles

Journal of Mass Spectrometry, Volume 61, Issue 8, August 2026.
ABSTRACT This study investigates the presence and quantification of phthalates released into mineral waters from virgin and recycled polyethylene terephthalate (PET) bottles. A green, solvent‐free analytical method based on solid‐phase microextraction (SPME) coupled with gas chromatography–mass spectrometry (GC/MS) was developed and validated to detect
Claudia Lino, Serena Indelicato, David Bongiorno, Fabio D'Agostino, Giuseppe Avellone   +4 more
wiley   +1 more source