Results 41 to 50 of about 2,590 (173)

Determination of Trace Amounts of Lead with ETAAS After Single Drop Microextraction and Dispersive Liquid Liquid Microextraction Methods

open access: yesE3S Web of Conferences, 2013
Two liquid-phase microextraction procedures, single-drop microextraction (SDME) and dispersive liquid–liquid microextraction (DLLME), have been developed for the determination of lead by electrothermal atomic absorption spectrometry (ETAAS). Both methods
Efeçınar M.   +2 more
doaj   +1 more source

Comparison of DLLME to other methods for the determination of β2-agonists.

open access: yes, 2015
Comparison of DLLME to other methods for the determination of β2-agonists.
Xiao-Ou Su (466120)   +4 more
core   +1 more source

Determination of Organochlorine Pesticides in Green Leafy Vegetable Samples via Fe3O4 Magnetic Nanoparticles Modified QuEChERS Integrated to Dispersive Liquid-Liquid Microextraction Coupled with Gas Chromatography-Mass Spectrometry

open access: yesJournal of Analytical Methods in Chemistry, 2021
A fast method based on Fe3O4 magnetic nanoparticles (Fe3O4 MNPs) modified QuEChERS integrated to dispersive liquid-liquid microextraction (DLLME) coupled with gas chromatography-mass spectrometry was established for the determination of 8 organochlorine ...
Ling Yu   +8 more
doaj   +1 more source

Green and efficient preconcentration of calcium channel blocker drugs in water using effervescence powder in syringe-assisted deep eutectic solvent dispersive liquid-liquid microextraction

open access: yesGreen Analytical Chemistry, 2023
Efficient preconcentration techniques are crucial for the analysis of calcium channel blocker drugs such as amlodipine and nifedipine, commonly used for hypertension and heart diseases.
Shohbah Tamilselvam   +3 more
doaj   +1 more source

Advanced Sorbent Materials in Solid‐Phase Extraction: A Decade of Innovation and Future Perspectives

open access: yesChemistry–Methods, Volume 6, Issue 8, August 2026.
This review systematically summarizes five families of advanced sorbent materials for solid‐phase extraction (SPE): nanocarbons, porous frameworks (MOFs/COFs), smart polymers, biomass‐derived sorbents, and multifunctional composites. Key molecular interactions (π–π stacking, hydrogen bonding, electrostatic attraction, host–guest recognition) are ...
Xingchen Wang   +4 more
wiley   +1 more source

Green and Rapid Determination of Phthalates in Mineral Water From Virgin and Recycled PET Bottles

open access: yesJournal of Mass Spectrometry, Volume 61, Issue 8, August 2026.
ABSTRACT This study investigates the presence and quantification of phthalates released into mineral waters from virgin and recycled polyethylene terephthalate (PET) bottles. A green, solvent‐free analytical method based on solid‐phase microextraction (SPME) coupled with gas chromatography–mass spectrometry (GC/MS) was developed and validated to detect
Claudia Lino   +4 more
wiley   +1 more source

Determination of Parabens in Breast Milk Samples by Dispersive Liquid-Liquid Microextraction (DLLME) and Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry

open access: yes, 2019
A reliable method was developed and validated based on dispersive liquid-liquid microextraction (DLLME) and ultra-high-performance liquid chromatography coupled to tandem mass spectrometry (UHPLC-MS/MS) to determine simultaneously methylparaben (MePB ...
Vinicius R. Acquaro Junior (6210497)   +3 more
core   +1 more source

Recent Advances in the Use of Natural Deep Eutectic Solvents for Natural Product Sample Preparation: Focus on Purification, Characterization, and Sustainability

open access: yesJournal of Separation Science, Volume 49, Issue 7, July 2026.
ABSTRACT This review examines recent advances in the use of natural deep eutectic solvents (NaDES) for natural product sample preparation, with emphasis on extraction, purification, analytical compatibility, and sustainability. NaDES emerge as versatile, tunable, and biocompatible media that enhance the recovery and stability of diverse phytochemicals ...
Valeria Cedeño‐Fierro   +3 more
wiley   +1 more source

A Natural Monoterpene Enol for Dispersive Liquid–Liquid Microextraction Based on Solidification of Floating Organic Droplets for Determination of Benzophenone Compounds in Water Samples

open access: yesSeparations, 2022
In the current study, an effective and simple procedure of extraction for the four benzophenone compounds from water samples was achieved by dispersive liquid–liquid microextraction (DLLME) based on the solidification of floating organic droplets (SFO ...
Xian Zhang   +7 more
doaj   +1 more source

Development of a Sustainable and Practical Natural Deep Eutectic Solvent‐based Ultrasound‐assisted Microextraction Method for Determining Fipronil and Its Degradation Products in Brewed Coffee

open access: yesJournal of Separation Science, Volume 49, Issue 5, May 2026.
ABSTRACT Fipronil and its degradation products, such as fipronil sulfide and fipronil desulfinyl, exhibit toxicological concerns and require reliable analytical methods for monitoring in complex matrices such as brewed coffee. This study aimed to develop a novel ultrasound‐assisted liquid–liquid microextraction approach using a natural deep eutectic ...
Natália Stram Bierhals   +4 more
wiley   +1 more source

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