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Organic Electrosynthesis: Applications in Complex Molecule Synthesis
ChemElectroChem, 2019 Organic electrosynthesis is an enabling and sustainable technology, which constitutes a rapidly expanding field of research. Electrochemical approaches serve as convenient and green alternatives to stoichiometric and toxic chemical redox agents ...
Andrey Shatskiy +2 more
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Electrosynthesis of Imidazolium Carboxylates
Organic Letters, 2013Synthesis of imidazolium carboxylate compounds was efficiently achieved by electrochemical reduction of imidazolium precursors under very mild conditions.
Guillaume, de Robillard +5 more
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Electrosynthesis ofN-Methylisatin
The Journal of Organic Chemistry, 2019Isatin in a solution of dry N,N-dimethylformamide/NaClO4 is electroreduced in the presence of CH3I. N-methylisatin (NMI) is obtained in quantitative molar yield and high current efficiency by controlled potential electrolysis (CPE). NMI and N-methylisatoic anhydride are the reaction products when CPE is performed in the absence of CH3I, but adding it ...
Jaime F. Martínez Suárez +5 more
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A genetic approach for microbial electrosynthesis system as biocommodities production platform
Bioresource Technology, 2017 Microbial electrosynthesis is a process that can produce biocommodities from the reduction of substrates with microbial catalysts and an external electron supply.
Kyung A Jung, Jong Moon Park
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An electrosynthesis of sulphones
Journal of Applied Electrochemistry, 1973The cathodic reduction of SO2, dissolved in aprotic solvents, to the anion radical SO2− in the presence of organic halides RX results in the formation of organic sulphones R-SO2-R at appreciable current yields. With dihalides, polymeric sulphones or, as in the case ofo-xylylenedibromide, inner sulphinic esters (sultines) are formed, the latter being ...
D. Knittel, B. Kastening
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Nature, 1985
Since Chatt and co-workers first reported that the protolysis of the dinitrogen complex cis-[W(N2)2(PMe2Ph)4] gives ammonia1, cis-[W(N2)2(PMe2Ph)4]H+→ 2NH3 + N2 + degradation products (1) there has existed the engaging possibility that a cyclic conversion of molecular nitrogen to ammonia might be achieved at room temperature and pressure using ...
Christopher J. Pickett, Jean Talarmin
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Since Chatt and co-workers first reported that the protolysis of the dinitrogen complex cis-[W(N2)2(PMe2Ph)4] gives ammonia1, cis-[W(N2)2(PMe2Ph)4]H+→ 2NH3 + N2 + degradation products (1) there has existed the engaging possibility that a cyclic conversion of molecular nitrogen to ammonia might be achieved at room temperature and pressure using ...
Christopher J. Pickett, Jean Talarmin
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Modeling Microbial Electrosynthesis
2017Mathematical modeling is an overarching approach for assessing the complexity of microbial electrosynthesis (MES) and for complementing the relevant experimental research. By describing and linking compartments, components, and processes with appropriate mathematical equations, MES and the corresponding bioelectrodes and complete bioelectrochemical ...
Benjamin, Korth, Falk, Harnisch
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Electrosynthesis of Protected Dehydroamino Acids
Organic Letters, 2023A NaCl-mediated electrochemical oxidation of amino acid carbamates (R1 = Boc, Cbz) afforded α-methoxylated α-amino acids. Subsequent acid-catalyzed elimination delivered valuable dehydroamino acid derivatives. The simplicity of our setup using graphite-electrodes was showcased, producing N-Boc-ΔAla-OMe on a decagram scale.
Marcel Gausmann +2 more
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Electrosynthesis of 1,2,4-Triazolium Tetrafluoroborates
Organic Letters, 2021The synthesis of 1,2,4-triazolium tetrafluoroborates under electrochemical conditions is reported. The reaction is performed with stoichiometric amounts of HBF4, which converts starting materials to their corresponding cationic forms due to protonation.
Marcin Budny +2 more
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ECS Meeting Abstracts, 2021
Owing to its many distinct characteristics, electrochemistry represents an attractive approach to discovering new reactions and meeting the prevailing trends in organic synthesis. Recently, we developed various new synthetic strategies that harness the power of electrochemistry for the functionalization of alkenes to access a diverse array of ...
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Owing to its many distinct characteristics, electrochemistry represents an attractive approach to discovering new reactions and meeting the prevailing trends in organic synthesis. Recently, we developed various new synthetic strategies that harness the power of electrochemistry for the functionalization of alkenes to access a diverse array of ...
openaire +1 more source