Results 141 to 150 of about 5,026 (252)

In Situ X‐Ray Diffraction Study of a Microwave‐Based Hydrothermal Synthesis of Mayenite Ca12Al14O33

open access: yesZeitschrift für anorganische und allgemeine Chemie, EarlyView.
Microwave‐assisted hydrothermal synthesis enables rapid transformation of aluminium‐ and calcium‐hydroxide into mayenite with high surface area. Optimised synthesis conditions comprise a microwave step at 80°C for 5 min followed by calcination at 800°C. The reactions during calcination were studied via in situ XRD measurements.
Nils L. Kotschote   +3 more
wiley   +1 more source

Microsecond X‐ray reflectometry

open access: yesJournal of Applied Crystallography, EarlyView.
X‐ray reflectometry is accelerated to 213 µs net exposure time using galvanometer scanning, which enables unprecedented temporal resolution for studying dynamic thin‐film processes.We accelerate synchrotron X‐ray reflectometry (XRR) by more than an order of magnitude and demonstrate the acquisition of full reflectivity curves within 213 µs over a qz ...
Michael Haberl   +6 more
wiley   +1 more source

NeuDiff Agent: a governed AI workflow for single‐crystal neutron crystallography

open access: yesJournal of Applied Crystallography, EarlyView.
NeuDiff Agent accelerates the TOPAZ single‐crystal neutron diffraction workflow at the Spallation Neutron Source from measured data to a structure suitable for publication through governed tool execution, auditable provenance and checkCIF assessment.Large‐scale facilities increasingly face analysis and reporting latency as a limiting step in scientific
Zhongcan Xiao   +3 more
wiley   +1 more source

Integrating measurement and simulation for evaluation of patient-specific whole-body dosimetry in clinical BNCT. [PDF]

open access: yesMed Phys
Kakino R   +11 more
europepmc   +1 more source

Mobile electromagnetic levitator for time‐resolved in situ X‐ray diffraction studies of high‐temperature phase transformations

open access: yesJournal of Synchrotron Radiation, EarlyView.
A mobile electromagnetic levitator combined with time‐resolved synchrotron X‐ray diffraction enables in situ studies of high‐temperature phase transformations without container‐induced contamination and reveals the first direct observation of metastable phase formation in undercooled Fe–Co alloys.In situ observations of high‐temperature transformations,
Olga Shuleshova   +6 more
wiley   +1 more source

Simulating neutron protein crystallography experiments: applications to the development of the NMX instrument at ESS

open access: yesActa Crystallographica Section D, EarlyView.
Monte Carlo simulations of neutron protein diffraction experiments provide useful data that models neutrons interacting with instrument components, as well as the crystal diffraction itself. These data can be applied to instrument development, such as the commissioning of the NMX Macromolecular Diffractometer at ESS.Monte Carlo neutron ray‐tracing ...
Mads Bertelsen   +7 more
wiley   +1 more source

Review of Radiation Embrittlement of Aluminum Alloys Used in Research Reactors. [PDF]

open access: yesMaterials (Basel)
Gillemot F   +4 more
europepmc   +1 more source

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