Results 151 to 160 of about 5,130 (292)

Decoding Carbon Dot Purity by Nuclear Magnetic Resonance

open access: yesAngewandte Chemie, EarlyView.
NMR spectroscopy tracks the removal of molecular and oligomeric impurities in carbon dots, enabling a (semi)quantitative evaluation of their purity through integrated peak analysis. ABSTRACT Carbon dots (CDs) have attracted increasing attention in recent years and have been widely explored in many fields.
Yalei Hu, Alberto Bianco
wiley   +2 more sources

Selective Electrolysis of Water Under Artificial Seawater Conditions Using Transition Metal Borate Anodes

open access: yesAdvanced Energy Materials, EarlyView.
The borate‐based cobalt‐iron catalyst promotes selective oxidation of water rather than chlorine evolution reaction during electrolysis of seawater. When integrated into a zero‐gap electrolyzer prototype, this catalyst supports robust splitting of artificial seawater into oxygen and hydrogen on an extended timescale.
Ananta R. Fareza   +10 more
wiley   +1 more source

One‐Step Radical‐Intensified Selective Etching (RISE) Strategy for High‐Yield Synthesis of Monolayer MXene with Tailored Nanoholes

open access: yesAngewandte Chemie, EarlyView.
Radical‐intensified selective etching (RISE) delivers monolayer MXenes with >80% yield in just 3 h etching process. Controlled ·OH dosage enables one‐step access to holey MXenes with abundant nanopores or defect‐lean flakes. This mild, safe strategy couple ultrafast kinetics with structural tunability, advancing precision design of MXene architectures.
Chenxu Liu   +8 more
wiley   +2 more sources

Suppressing Dendrite Formation through Au‐Driven Interfacial Engineering for Solid‐State Lithium‐Metal Batteries

open access: yesAdvanced Energy Materials, EarlyView.
A thin gold nanolayer on lithium metal enables stable and uniform lithium plating in solid‐state batteries, enabling nearly 1 year and 11 months of continuous operation. The conductive coating lowers interfacial resistance, suppresses dendrite growth, and improves cycling stability, attributed to homogeneous deposition of Li+ on the gold layer ...
Natalia Voronina   +10 more
wiley   +1 more source

Convergent Valorization via Scalable C═N Bond Electrosynthesis Through Metal‐Dopant Interfacial Engineering in a Flow Electrolyzer

open access: yesAngewandte Chemie, EarlyView.
This study establishes an innovative approach to synthesize organonitrogens featuring C═N bonds efficiently using non‐precious metal‐doped MoS2 in a flow electrolyzer. Fe dopant significantly enhances Faradaic efficiency and yield rate, achieving over 81% and 2630 mmol h−1 g−1 for formaldoxime production. This platform upcycles pollutants into valuable
Ruijie Yi   +9 more
wiley   +2 more sources

Bayesian Optimisation for the Experimental Sciences: A Practical Guide to Data‐Efficient Optimisation of Laboratory Workflows

open access: yesAdvanced Intelligent Systems, EarlyView.
This study provides an introduction to Bayesian optimisation targeted for experimentalists. It explains core concepts, surrogate modelling, and acquisition strategies, and addresses common real‐world challenges such as noise, constraints, mixed variables, scalability, and automation.
Chuan He   +2 more
wiley   +1 more source

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