Results 211 to 220 of about 354,183 (253)
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In-syringe solid-phase extraction of polycyclic aromatic hydrocarbons using an iron–carboxylate metal–organic framework and hypercrosslinked polymer composite gelatin cryogel–modified cellulose acetate adsorbent

Microchimica Acta, 2022
Cellulose acetate fibers were modified with a gelatin cryogel adsorbent incorporating an iron-carboxylate metal-organic framework and hypercrosslinked polymer composite. The hybrid adsorption materials facilitated the adsorption ability toward polycyclic aromatic hydrocarbons and were entrapped into gelatin cryogel to be hierarchically coated on ...
Suppawan Sillapawisut   +3 more
openaire   +2 more sources

Combination of Syringe–Solid Phase Extraction with Inductively Coupled Plasma Mass Spectrometry for Efficient Heavy Metals Detection

CLEAN – Soil, Air, Water, 2016
This work aimed to combine solid phase extraction (SPE) with inductively coupled plasma mass spectrometry for the determination of multi‐elements (Pb, Cd, and Zn) simultaneously. This combination allows the purification of the solution by minimizing matrix effects, the separation of the analytes and a fast determination of multiple elements (Pb, Cd ...
ALOthman, Zeid A.   +3 more
openaire   +2 more sources

Thin-layer chromatography of some metals on silica gel layers impregnated with salicylic, syringic and o-phthalic acid

Journal of Chromatography A, 1990
Etude du comportement chromatographique de certains metaux (Co, Cu, Fe, Hg, Pb) sur des couches minces de gel de silice impregnees par des acides en utilisant des eaux de distribution et distillee comme ...
I. Škvorc   +3 more
openaire   +1 more source

An automatic stirring-assisted liquid–liquid microextraction system based on lab-in-syringe platform for on-line atomic spectrometric determination of trace metals

Talanta, 2017
A novel simple fully automatic on-line magnetic stirring-assisted liquid-liquid microextraction method, based on the lab-in-syringe (LIS) concept, has been developed as an alternative approach for sample pretreatment and atomic spectrometric assays. The analytical process includes the in-syringe reaction of the metal ion with the chelating reagent, the
Georgia, Giakisikli   +1 more
openaire   +2 more sources

Facile preparation of metal organic framework-based laboratory semi-automatic micro-extraction syringe packed column for analysis of parabens in vegetable oil samples

Microchemical Journal, 2020
Abstract A simple and efficient integrated, laboratory-made, semi-automatic microextraction packed in a syringe (Semi-automated MEPS) was first assembled and validated for the extraction of parabens in vegetable oils. Several representative metal–organic frameworks were prepared and used as sorbents for the direct extraction of analytes from diluted ...
Yanxiao Jiang   +8 more
openaire   +1 more source

Metal–organic framework based in‐syringe solid‐phase extraction for the on‐site sampling of polycyclic aromatic hydrocarbons from environmental water samples

Journal of Separation Science, 2018
AbstractIn‐syringe solid‐phase extraction is a promising sample pretreatment method for the on‐site sampling of water samples because of its outstanding advantages of portability, simple operation, short extraction time, and low cost. In this work, a novel in‐syringe solid‐phase extraction device using metal–organic frameworks as the adsorbent was ...
Xiaoqiong Zhang   +5 more
openaire   +2 more sources

Application of metal-organic framework MIL-101(Cr) to microextraction in packed syringe for determination of triazine herbicides in corn samples by liquid chromatography-tandem mass spectrometry

Journal of Chromatography A, 2018
In this work, a metal-organic framework material MIL-101(Cr) was prepared and used as the sorbent for a laboratory-made semi-automated microextraction in packed syringe (MEPS). Six triazine herbicides, including desmetryn, prometon, ametryn, prometryn, atraton, and dipropetryn, that are commonly found in corn samples, were extracted and determined by ...
Yanxiao Jiang   +7 more
openaire   +2 more sources

Experimental (FT-IR, FT-Raman, 1H, 13C NMR) and theoretical study of alkali metal syringates

Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 2013
In this work the influence of lithium, sodium, potassium, rubidium and cesium on the electronic system of the syringic acid (4-hydroxy-3,5-dimethoxybenzoic acid) was studied. This paper presents spectroscopic vibrations (FT-IR, FT-Raman) and NMR ((1)H and (13)C) study of the series of alkali metal syringates from lithium to cesium syringates ...
openaire   +2 more sources

A continuous flow polyurethane foam solid phase microextraction lab-in-syringe platform for the automatic determination of toxic metals

Talanta
A novel fully automatic continuous flow polyurethane foam solid phase microextraction lab-in-syringe system for on-line sample preconcentration/separation has been developed as a front-end to flame atomic absorption spectrometry. For the first time lab-in-syringe in continuous flow has been adopted for the determination of toxic metals.
Natalia, Manousi, Aristidis, Anthemidis
openaire   +2 more sources

Environmentally sustainable needle hub in-syringe μ-SPE method using metal-organic gel for on-site extraction of polycyclic aromatic hydrocarbons in water samples

Talanta
A green, simple, low-cost, miniaturized, and portable needle hub-in-syringe micro solid phase extraction (NH-IS-μ-SPE) method was developed using a green metal-organic gel (MOG) sorbent. Coupled with high-performance liquid chromatography diode array detector (HPLC-DAD), this approach enables efficient extraction and preconcentration of seven selected ...
Xin Ai Wong   +3 more
openaire   +2 more sources

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