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Direct detection of mercury in vapor and aerosol from chemical atomization and nebulization at ambient temperature: exploiting the flame atomic absorption spectrometer

Journal of Analytical Atomic Spectrometry, 2005
A Y-shaped Teflon connector was designed to branch the capillary of a conventional commercial flame atomic absorption spectrometer for the introduction of inorganic Hg2+ aqueous solution and KBH4 solution. The two solutions were merged inside the connector before being nebulized into an aerosol by air in the nebulizer of the instrument, and the atomic ...
Qiuju Yang   +4 more
openaire   +1 more source

Thickness dependence of microstructure and properties of ZnO thin films deposited by metal-organic chemical vapor deposition using ultrasonic nebulization

Thin Solid Films, 2013
Abstract ZnO thin films were deposited on soda lime glass substrates at 275 °C by metal-organic chemical vapor deposition using ultrasonic nebulization and the dependence of their microstructures and properties on film thickness were investigated. Deposition rate was controlled by mass transfer rate at flow rates lower than 6 l/min and by surface ...
Choon-Ho Lee, Do-Woo Kim
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An in-depth evaluation of accuracy and precision in Hg isotopic analysis via pneumatic nebulization and cold vapor generation multi-collector ICP-mass spectrometry

Analytical and Bioanalytical Chemistry, 2015
Mercury (Hg) isotopic analysis via multi-collector inductively coupled plasma (ICP)-mass spectrometry (MC-ICP-MS) can provide relevant biogeochemical information by revealing sources, pathways, and sinks of this highly toxic metal. In this work, the capabilities and limitations of two different sample introduction systems, based on pneumatic ...
Ana, Rua-Ibarz   +2 more
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Effects of the Ga-doping concentration on the characteristics of Zn0.7Mg0.3O thin films deposited by metal-organic chemical vapor deposition using an ultrasonic nebulization

Journal of Electroceramics, 2018
Ga-doped Zn0.7-xMg0.3O thin films were deposited on glass substrates at 350 °C by metal-organic chemical vapor deposition using an ultrasonic nebulization technique to transport the source precursors, and the effects of the Ga-doping concentration were investigated.
Choon-Ho Lee, Min-Seok Choi
openaire   +1 more source

Determination of Mercury Compounds in Water Samples by Liquid Chromatography–Inductively Coupled Plasma Mass Spectrometry With anIn Situ Nebulizer/Vapor Generator

J. Anal. At. Spectrom., 1997
A preliminary study of a cold vapor generation system as the sample introduction device for liquid chromatography–inductively coupled plasma mass spectrometry (LC–ICP-MS) is described. Samples containing ionic mercury compounds were subjected to chromatographic separation before injection into the cold vapor generator.
CHIA-CHING WAN   +2 more
openaire   +1 more source

In situ vapor generation inductively coupled plasma spectrometry for determination of iodine using a triple-mode microflow ultrasonic nebulizer after alkaline solubilization

Analytical Methods, 2010
The analytical potential of a coupled continuous-microflow ultrasonic nebulizer triple-mode micro-capillary system (µ-USN/TCS) for the determination of iodine in biological samples by direct iodine vapor generation inductively coupled plasma optical emission spectrometry (VG-ICP-OES) has been investigated.
Henryk Matusiewicz   +1 more
openaire   +1 more source

Improved determination of iodine by sequential (photo)chemical vapor generation and pneumatic nebulization in the programmable temperature spray chamber and inductively coupled plasma optical emission spectrometry

Microchemical Journal, 2014
Abstract Continuous generation of volatile iodine species based on chemical or photochemical oxidation may be further improved using a sequential (photo)chemical vapor generation/pneumatic nebulization/programmable-temperature spray chamber (P)CVG–PN–PTSC system providing the benefits of a temperature-controlled ICP sample introduction technique. Two
K. Jankowski, J. Giersz, M. Paprocka
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Ultrasonic Nebulization, Multimode Sample Introduction System for Simultaneous Determination of Hydride-Forming, Cold Vapor, and Non-Hydride-Forming Elements by Microwave-Induced Plasma Spectrometry

Spectroscopy Letters, 2014
ABSTRACT A novel synergic effect of ultrasonic nebulization (USN) and a multimode sample introduction system (MSIS) when used in combination has been exploited for efficient generation of conventional hydride-forming (As, Bi, Ge, Sb, Se, Sn), Hg vapor, and non-hydride-forming (Ba, Ca, Li, Mg, Sr) elements. The ultrasonic nebulizer supplied a microliter
Henryk Matusiewicz   +1 more
openaire   +1 more source

Sensitive determination of Hg together with Mn, Fe, Cu by combined photochemical vapor generation and pneumatic nebulization in the programmable temperature spray chamber and inductively coupled plasma optical emission spectrometry

Talanta, 2017
Continuous photo-induced generation of mercury cold vapor has been successfully coupled with conventional pneumatic nebulization in programmable temperature spray chamber (PCVG-PN-PTSC) allowing fast, sensitive and easy multi-element analysis. The applied technique enabled simultaneous determination of non-volatile forming elements (Fe, Cu, Mn) and ...
Jacek, Giersz   +2 more
openaire   +2 more sources

Ultrasonic Nebulization/UV Photolysis Vapor Generation Sample Introduction System for the Determination of Conventional Hydride (As, Bi, Sb, Se, Sn) and Cold Vapor (Hg, Cd) Generation Elements in Reference Materials in the Presence of Acetic Acid by Microwave-Induced Plasma Spectrometry

Spectroscopy Letters, 2013
ABSTRACT A novel synergic effect of ultrasonic nebulization (USN) and ultraviolet (UV) radiation (photolysis) when used in combination has been exploited for efficient generation of conventional hydride elements (As, Bi, Sb, Se, Sn), Hg vapor, and volatile molecular Cd species.
H. Matusiewicz, M. Ślachciński
openaire   +1 more source

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