Results 201 to 210 of about 65,368 (313)

Microsecond X‐ray reflectometry

open access: yesJournal of Applied Crystallography, EarlyView.
X‐ray reflectometry is accelerated to 213 µs net exposure time using galvanometer scanning, which enables unprecedented temporal resolution for studying dynamic thin‐film processes.We accelerate synchrotron X‐ray reflectometry (XRR) by more than an order of magnitude and demonstrate the acquisition of full reflectivity curves within 213 µs over a qz ...
Michael Haberl   +6 more
wiley   +1 more source

NeuDiff Agent: a governed AI workflow for single‐crystal neutron crystallography

open access: yesJournal of Applied Crystallography, EarlyView.
NeuDiff Agent accelerates the TOPAZ single‐crystal neutron diffraction workflow at the Spallation Neutron Source from measured data to a structure suitable for publication through governed tool execution, auditable provenance and checkCIF assessment.Large‐scale facilities increasingly face analysis and reporting latency as a limiting step in scientific
Zhongcan Xiao   +3 more
wiley   +1 more source

Mobile electromagnetic levitator for time‐resolved in situ X‐ray diffraction studies of high‐temperature phase transformations

open access: yesJournal of Synchrotron Radiation, EarlyView.
A mobile electromagnetic levitator combined with time‐resolved synchrotron X‐ray diffraction enables in situ studies of high‐temperature phase transformations without container‐induced contamination and reveals the first direct observation of metastable phase formation in undercooled Fe–Co alloys.In situ observations of high‐temperature transformations,
Olga Shuleshova   +6 more
wiley   +1 more source

High‐flux, moderate‐bandwidth, high‐energy X‐rays from lapped Si(111) crystals in a double‐crystal monochromator

open access: yesJournal of Synchrotron Radiation, EarlyView.
Lapped Si(111) crystals in a double‐crystal monochromator provide high‐flux, spectrally pure, and moderate‐bandwidth X‐ray beams at 100 keV, offering a robust and cost‐effective alternative to perfect‐crystal and multilayer optics.Lapping the surfaces of Si(111) crystals in a double‐crystal monochromator significantly increases the intensity of high ...
Hiroshi Yamazaki   +3 more
wiley   +1 more source

Deciphering unusually large modulations in two related organic hydroxy channel structures

open access: yesActa Crystallographica Section B, EarlyView.
Two related organic hydroxy‐channel compounds are shown to have unusually large structural modulations.The incommensurately modulated structures of two related organic hydroxy‐channel compounds [(R)‐1‐(1,3‐dihydroxypropan‐2‐yl)‐3‐(octan‐2‐yl)urea, 1; 1‐(1,3‐dihydroxypropan‐2‐yl)‐3‐octylurea, 2] have been determined and compared to the structure of a ...
Arie van der Lee   +8 more
wiley   +1 more source

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