Results 21 to 30 of about 4,484,038 (290)

Vacuum-assisted headspace solid-phase microextraction and gas chromatography coupled to mass spectrometry applied to source rock analysis

open access: yesAdvances in Sample Preparation, 2022
Vacuum-assisted headspace solid phase microextraction (Vac-HSSPME) with high temperature of extraction was used for source-rock analysis. Optimization of extraction conditions was performed by Doehlert experimental design (DD) in gas chromatography ...
Breno J. Pollo   +4 more
doaj   +1 more source

Atomic spectrometry update. Clinical and biological materials, foods and beverages [PDF]

open access: yes, 2013
This review discusses developments in elemental mass spectrometry, atomic absorption, emission and fluorescence, XRF and LIBS, as applied to the analysis of specimens of clinical interest, foods and beverages.
Day, Martin P.   +5 more
core   +2 more sources

Application of solid-phase microextraction in atomic spectrometry

open access: yesAdvances in Sample Preparation, 2022
With the growing requirements for the monitoring of heavy metals at an ultra-trace level in the environment and the real-time detection of toxic elements and their compounds for environmental pollution accidents, researchers devoted significant efforts ...
Yubin Su   +3 more
doaj   +1 more source

An efficient configuration for simultaneous electromembrane extraction of acidic and basic drugs on a chip

open access: yesAdvances in Sample Preparation, 2022
In the present study, a new chip was designed for simultaneous electromembrane extraction (EME) of acidic and basic analytes. The method followed by the HPLC-UV analysis, was used for simultaneous extraction and determination of trace amounts of target ...
Zohre Hashemlou   +2 more
doaj   +1 more source

A review of sample preparation and its influence on pH determination in concrete samples [PDF]

open access: yes, 2017
If we are to monitor the chemical processes in cementitious materials, then pH assays in the pore solutions of cement pastes, mortars, and concretes are of key importance.
Aguado de Cea, Antonio   +1 more
core   +2 more sources

A comprehensive review on the use of microextraction techniques in the analysis of cosmetic products

open access: yesAdvances in Sample Preparation, 2022
Microextraction techniques have gained special relevance since their appearance in the 90s, and the analysis of cosmetic products has not been immune to this trend.
Lorenza Schettino   +3 more
doaj   +1 more source

Uncertainties of size measurements in electron microscopy characterization of nanomaterials in foods [PDF]

open access: yes, 2015
Electron microscopy is a recognized standard tool for nanomaterial characterization, and recommended by the European Food Safety Authority for the size measurement of nanomaterials in food.
Boxall, A. B. A.   +6 more
core   +1 more source

A Tutorial on AGREEprep an Analytical Greenness Metric for Sample Preparation

open access: yesAdvances in Sample Preparation, 2022
Sample preparation is a key step in the analytical procedure and a critical component for achieving analytical greenness. AGREEprep is the first metric intended for evaluating the environmental impact of sample preparation methods.
Francisco Pena-Pereira   +3 more
doaj   +1 more source

Pipette tip-electrospray mass spectrometry for determining opioids in urine, from on-site micro-handling to high-throughput centrifugal microextraction

open access: yesAdvances in Sample Preparation
Pipette tip-electrospray is a useful technique that synergically combines sample preparation and ambient ionization mass spectrometry for the rapid analysis of samples.
Jaime Millán-Santiago   +2 more
doaj   +1 more source

An effective palynological preparation procedure using hydrogen peroxide [PDF]

open access: yes, 2007
Most pre-Quaternary palynology samples are currently prepared by demineralization of the sediment/sedimentary rock matrix using hydrochloric and hydrofluoric acids (HCl and HF respectively).
Kyffin-Hughes, Jane E.   +2 more
core   +2 more sources

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