Carbon Nanomaterial Produced by Microwave Exfoliation of Graphite Oxide [PDF]
Carbon-based graphene-like material was obtained through microwave stimulated exfoliation of graph-ite oxide (GO). Properties of this material were investigated by multiple techniques including element analysis, X-ray photoelectron spectroscopy (XPS ...
Agapov, A.L. +9 more
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Ionothermal Synthesis of Sulfido‐Antimony Dicubanes with 3d‐Metal Spiro‐Atoms
The Lewis‐acidic ionic liquid [BMIm]Cl·4.4AlCl3 activates Sb2S3. With MCl2 (M = Fe, Co, Ni), dicubanes (MSb6S8)4+ can be crystallized. These clusters consist of two cubes that share one vertex, the spiro‐atom M. Counteranions are either [AlCl4]– or the novel group [S(AlCl3)4]2–. All three compounds are paramagnetic. Their optical band gaps range from 1.
Oliver Dreimann, Michael Ruck
wiley +1 more source
Catalytic and conductivity studies in two dimensional coordination polymers built with a thiazole based ligand [PDF]
The employment of the commercial availiable organic ligand 2-mercapto-4-methyl-5-thiazoleacetic acid (H2L) in Zn and Cd chemistry yields two-dimensional (2D) coordation polymers (CPs) with pseudopolymorphic character.
Abbasi +39 more
core +1 more source
Series of Microporous Redox‐Active Pillared Metal–Organic Frameworks Based On Alloxazine Ligands
Two series of robust pillared metal–organic frameworks using a redoactive ligand based on alloxazine and transition metals have been evidenced by XRD. The compounds have high decomposition temperatures, and their sorption properties are measured, revealing relatively low surface areas and a moderate uptake of CO2 and C2H4 at high pressures.
Jaison Casas +5 more
wiley +1 more source
A new sulfoxide analog of 1,2,3,6-tetrahydrophenylpyridine and antimicrobial activity [PDF]
Bioactivities of thiotetrahydropyridines were previously described. Herein, a novel bioactive sulfoxide analog; N-acetyl-2-(1-adamantylsulfoxo)-3-acetoxy-4-phenyl-6-hydroxy-1,2,3,6-tetrahydropyridine (3) from the deoxydative substitution of 4 ...
Pingaew, Ratchanok +4 more
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The crystal structures of (Ba6Nx)2[MN4][CN2]6 (left) and “ideal” 2 × 2 × 2 Perovskite (right) show similar linkage patterns despite differently shaped coordination polyhedra. Cubic carbodiimide nitride nitridometalates (Ba6Nx)2[MN4][CN2]6 of M = Zr, Hf, Nb, Ta, Mo, and W are synthesized by various high‐temperature reactions and their respective crystal
Peter Höhn +4 more
wiley +1 more source
ANÁLISE DE MEDICAMENTOS CONTENTO CLORIDRATO DE CICLOBENZAPRINA POR ESPECTROSCOPIA NO INFRAVERMELHO
O cloridrato de ciclobenzaprina é um dos medicamentos mais utilizados para atuar no relaxamento muscular e alivio de dores agudas ou crônicas, promovendo uma diminuição nos espasmos musculares, torcicolos e dor lombar. Este trabalho propõe-se a analisar,
Willian de Carvalho Nunes +1 more
doaj +1 more source
Influence of the degree of hydrolysis of poly(vinyl alcohol) on the physical properties of films based on blends of gelatin and poly(vinyl alcohol) plasticized with glycerol [PDF]
O objetivo deste trabalho foi o estudo do efeito do Grau de Hidrólise (GH) do poli(vinil álcool) (PVA) nas propriedades dos filmes à base de blendas de gelatina suína e PVA com dois GH.
BERGO, Paulo Victor de Albuquerque +5 more
core +2 more sources
The ultra‐alkaline condition of a hydroflux facilitate the synthesis of a new periodato cuprate(II). Fully deprotonated orthoperiodate octahedra are connected into chains by copper(II) cations. The two modifications differ in the constitution of these chains, which influences the magnetism of the compounds.
Huanyu He, Ralf Albrecht, Michael Ruck
wiley +1 more source
KENDALI PASAR DALAM PEMBERITAAN DI TELEVISI SWASTA NASIONAL (Analisis Wacana pada Berita Politik di 3 News Room: SCTV, Trans TV, dan Metro TV) [PDF]
Penelitian ini bertujuan mengidentifikasi keterkaitan antara kendali pasar dengan pemberitaan di televisi, dilihat dari aspek‐aspek kepentingan investor, sumber‐sumber berita, pengiklan dan konsumen atau penonton.
Agung, Machyudin
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