Results 1 to 10 of about 3,960 (103)
Background – Oral and parenteral drug delivery in horses can be difficult. Equine‐specific transdermal drug formulations offer improved ease of treatment; development of such formulations requires a deeper understanding of the structural and chemical tissue barrier of horse skin. Hypothesis/Objectives – To compare the structural composition and barrier
Samuel C. Bizley +3 more
wiley +1 more source
Highlights For the first time, our study contributed a systematic evaluation of bile acid (BA) profiles in plasma, feces and liver tissue and gut microbiota changes triggered by fasting‐refeeding cycle in mice. Our work clearly demonstrated that overnight fasting leads to significant, but reversible changes in BA profiles and gut microbiota composition.
Yi Zhang +16 more
wiley +1 more source
Background – Ceftazidime (CAZ) solutions are being used based on anecdotal reports for otitis externa complicated by multidrug‐resistant Pseudomonas aeruginosa (MDR PA). The chemical and microbiological stability of these proposed compounded solutions have not been evaluated, and likely are affected by the diluent and storage duration or temperature ...
Sarah E. Hoff +4 more
wiley +1 more source
Purification and Composition Analysis of Non-Extractable Polyphenols in Blueberry(蓝莓不可萃取多酚的纯化及组分分析) [PDF]
The extraction, separation and purification of non-extractable polyphenols (NEPP) in blueberries were studied and its components were analyzed using HPLC.The results showed that adsorption and desorption rates of HPD-100C were relatively high among seven
HAN Caijing(韩彩静) +5 more
doaj +1 more source
Effect of Secondary Distillation on Antimicrobial and Antioxidant Activities of Bamboo Vinegar(二级蒸馏对竹醋液抑菌与抗氧化效果的影响) [PDF]
The antimicrobial activities, free radical scavenging capacity, the content of total phenols, and total flavonoids of primary and secondary distilled bamboo vinegar were investigated. In addition, the primary and secondary distillation bamboo vinegar was
AN Lin(安 琳) +3 more
doaj +1 more source
采用高效液相色谱法(HPLC)、气相色谱质谱联用法(GC-MS/MS)以及液相色谱质谱联用法(HPLCMS/ MS)测定动物源性食品中镇静剂类药物地西泮的残留量。将样品均质粉碎后,经乙腈提取,固相萃取小柱净化后上机检测,外标法定量。实验证明,当固相萃取的洗脱液中甲醇与乙酸溶液的体积比为70:30 时,洗脱效率最高。在不同仪器条件下,地西泮在各自浓度范围内的线性关系良好,相关系数(r2) 均大于0.999,回收率在 84.6%~ 101.7%,相对标准偏差(RSD) 在0.52%~9.44% (n=3 ...
DINGYuqi(丁宇琦) +3 more
doaj +1 more source
为快速、准确监测水产养殖环境水体中孔雀石绿含量,建立了一种超高效液相色谱-串联质谱法(UPLC-MS/MS)测定水产养殖水体中孔雀石绿及隐色孔雀石绿的方法.水样经甲酸酸化预处理后,采用多壁碳纳米管固相萃取柱富集和净化目标物,超高效液相色谱分离,三重四级杆质谱检测,氘代同位素内标定量.在优化条件下,孔雀石绿和隐色孔雀石绿在0. 02~10. 0 µg • L-1浓度范围内均满足线性关系,相关系数R2>0. 998,方法检出限、定量限分别为0. 000 3和0. 001 µg • L-1.在0. 005~0.
MEIGuangming(梅光明) +6 more
doaj +1 more source
Determination of Maleic Acid and Fumaric Acid in Starch and Starch Products Using SPE-UHPLC Method(SPE-UHPLC测定淀粉及淀粉制品中丁烯二酸类酸度调节剂) [PDF]
In the present study, a solid-phase extraction ultra high performance liquid chromatographic(UHPLC)method was established for the analysis of maleic acid, fumaric acid, and maleic anhydride in starch and starch products. Starch samples were cleaned up by
BIE Wei(别 玮) +3 more
doaj +1 more source
建立了超高效液相色谱串联质谱法测定水产品中的红霉素残留量.样品用改进的QuEChERS(快速、简单、廉价、高效、灵活和安全)进行提取净化,经乙腈快速提取,无水硫酸镁和氯化钠除水后,用N-丙基乙二胺(PSA)净化,液相色谱串联质谱分析测定.在ACQUITY UPLC BEH C18色谱柱上进行分离,采用梯度洗脱,以0.1%甲酸水溶液和甲醇为流动相,电喷雾正离子电离,多反应监测模式,内标法定量.结果表明:红霉素浓度在0.5~50 µg • L-1时具有良好的线性关系,相关系数为0.997 6,定量限为0.3
YANZhongyong(严忠雍) +7 more
doaj +1 more source
Thermal stability of hydrocarbon fuel under supercritical condition(碳氢燃料的超临界热稳定性研究)
以正壬烷为碳氢燃料模型化合物,考察其在超临界条件下的恒容热裂解,跟踪裂解转化率和产物分布,探讨了反应温度和时间对燃料热稳定性的影响.正壬烷热裂解气体产物主要有甲烷、乙烷、乙烯、丙烷和丙烯;液态产物中则以链烷烃、烯烃和环烷烃为主,并可检测到芳烃.采用高效液相色谱(HPLC)法测定了液体产物中芳烃的含量,与气相色谱-质谱联用(GC-MS)和紫外-可见光谱(UV-vis)测定结果相互印证,芳烃含量随裂解转化率增加呈指数变化,表达了燃料热稳定性和裂解规律的变化趋势.
QINXiao-mei(秦笑梅) +4 more
doaj +1 more source

