Results 71 to 80 of about 1,079,697 (312)

Surprising Water Slipping Performance on Highly Hydrophilic PEG‐Derived Monolayer‐Covered Surfaces: Preparation, Mechanism, and Application

open access: yesAdvanced Functional Materials, EarlyView.
Highly hydrophilic surfaces (water contact angle, ≈17.7°) exhibiting surprising water slipping performance (sliding angle, ≈7.3°) are successfully prepared via simple chemisorption of polyethylene glycol (PEG) organosilane and subsequent alkali‐treatment.
Hyeonjin Kim   +5 more
wiley   +1 more source

A Gallium-based Chiral Solvating Agent Enables the Use of 1H NMR Spectroscopy to Differentiate Chiral Alcohols

open access: yesiScience, 2019
Summary: In situ, direct 1H NMR chiral analysis by using chiral solvating agents is a convenient and efficient analytical technique. Here we developed a Ga-based chiral anionic metal complex for 1H NMR chiral analysis of alcohols.
Sumin Jang, Hyunwoo Kim
doaj   +1 more source

Coupling Anodic Activity and Stability at Ni‐Based Non‐Oxide Catalysts via Coordinating Alcohol Oxidation and Oxygen Evolution

open access: yesAdvanced Functional Materials, EarlyView.
A cooperative and competitive interrelationship between alcohol oxidation (AOR) and water oxidation (OER) was observed on a typical anode catalyst of Ni2P. In situ Raman spectroscopy and electrochemical analyses revealed a specific complementary mechanism between them, in which OER and AOR critically contribute to the activity and stability of anodic ...
Yong Yan   +10 more
wiley   +1 more source

An NMR Study on Prucalopride

open access: yesChinese Journal of Magnetic Resonance, 2018
4-Amino-5-chloro-2,3-dihydro-N-[1-(3-methoxypropyl)-4-piperidinyl]-7-benzofurancarboxamide was synthesized by amide condensation reaction using 4-amino-5-chloro-2,3-dihydrobenzofuran-7-carboxylic acid and 1-(3-methoxypropyl)- 4-piperidinamine as the ...
ZHOU Zhong-gao   +4 more
doaj   +1 more source

Authentication of beef versus horse meat using 60 MHz 1H NMR spectroscopy

open access: yesFood Chemistry, 2015
Highlights • Demonstration of 60 MHz 1H NMR as a screening tool for distinguishing beef from horse meat.• A simple chloroform extraction combined with a 10 min spectral acquisition time.• A principal components-based authenticity model yielding a ‘beef ...
W. Jakes   +8 more
semanticscholar   +1 more source

Bio‐Inspired Synthesis of Macroporous Single Crystal Particles as Scattering Agents

open access: yesAdvanced Functional Materials, EarlyView.
A general strategy is presented that delivers unique, single‐crystal microparticles that combine submicron macroporosity and uniform particle shapes. A bioinspired approach is used to occlude three distinct types of additives – polystyrene microspheres, polymer vesicles and amino acids – within calcite single crystals, and subsequent thermal annealing ...
Stephanie E. Foster   +11 more
wiley   +1 more source

An NMR Study on Esculetin and It's Derivatives

open access: yesChinese Journal of Magnetic Resonance, 2019
The derivatives of esculetin contain hydroquinone groups that have various biological activities. In this study, the esculetin derivatives 2~14 were obtained by inducting the methoxy and hydroxyl groups into the 5, 6, 7 and 8 positions, and pheny group ...
LIU Ji-hong, JIN Kun, WANG Ping, LUO Gen
doaj   +1 more source

A 1H NMR relaxometry investigation of gel-pore drying shrinkage in cement pastes

open access: yes, 2016
The first systematic study of the temporal evolution of the pore-size-distribution (PSD) in mature cement pastes following one and two cycles of drying and rewetting is presented. The PSD is measured using 1H nuclear magnetic resonance (NMR) relaxometry.
A. Gajewicz   +4 more
semanticscholar   +1 more source

Shape Memory Microneedle to Prevent Risks of Reproductive Hormone Therapy by Switching Sustained to Burst Release Under a Single Transdermal Insertion

open access: yesAdvanced Functional Materials, EarlyView.
A shape‐memory microneedle system enables reproductive hormone therapy through a single transdermal insertion. The X‐shaped device sustains follicle‐stimulating hormone release for three days, and mild heating restores the O shape to trigger burst human chorionic gonadotropin release.
Sungwoo Cho   +8 more
wiley   +1 more source

1H-NMR as a Structural and Analytical Tool of Intra- and Intermolecular Hydrogen Bonds of Phenol-Containing Natural Products and Model Compounds

open access: yesMolecules, 2014
Experimental parameters that influence the resolution of 1H-NMR phenol OH signals are critically evaluated with emphasis on the effects of pH, temperature and nature of the solvents.
P. Charisiadis   +5 more
semanticscholar   +1 more source

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