Results 1 to 10 of about 208,364 (208)
Separation performance of PEG-linked calix[4]arene as stationary phase for capillary gas chromatography [PDF]
This work presented a new PEG modified calix[4]arene stationary phase (C4A-PEG-2PTSC) for gas chromatographic (GC) separations. The statically coated C4A-PEG-2PTSC column exhibited moderate polarity and column efficiency of 2224 plates m-1 determined by ...
Wei Zhang +8 more
doaj +1 more source
Analysis of α-lipoprotein cholesterol in 50 μl of plasma
A micromethod for quantitation of α-lipoprotein cholesterol was devised for gas–liquid chromatography to minimize plasma sample size and facilitate lipid studies using capillary blood from children or small animals. α-Lipoprotein cholesterol was measured
R.F. Lutmer +7 more
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Accelerated gas-liquid visible light photoredox catalysis with continuous-flow photochemical microreactors [PDF]
In this protocol, we describe the construction and use of an operationally simple photochemical microreactor for gas-liquid photoredox catalysis using visible light.
A Günther +26 more
core +3 more sources
Rapid determination of methylmercury in fish tissues
The aim of the present study was to develop a rapid and inexpensive method for the determination of methylmercury in fish tissues based on GC/ECD instrumentation.
Petr Maršálek, Zdeňka Svobodová
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Recent developments in the rapid analysis of plants and tracking their bioactive constituents [PDF]
Natural products chemistry has witnessed many new developments in the last 5 years like extractions with subcritical water and ionic liquids, LC/HRMS and LC/SPE/cryo-NMR, UHPLC, TLC/MS, MS-based preparative HPLC, comprehensive chromatography (GC × GC, LC
Beek, T.A., van +7 more
core +2 more sources
Determination of lipid content and fatty acid representation in barley caryopses and malt.
The modern method of extraction on the fluidized bed was optimized for the determination of lipids in barley caryopses and malt. Representation of fatty acids in barley caryopsis and malt was determined from extracted lipids.
Zdeněk SVOBODA +4 more
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Determination of gamma-hydroxybutyric acid in dried blood spots using a simple GC-MS method with direct 'on spot' derivatization [PDF]
The objective of this study was the development of an accurate and sensitive method for the determination of gamma-hydroxybutyric acid (GHB) in dried whole blood samples using a GC-MS method.
Ingels, Ann-Sofie +2 more
core +1 more source
Capillary gas-liquid chromatographic separation was studied for the complete set of the 26 theoretically possible isomers of mono-, di-, and trihydroxylated 5 beta-cholanic acids, which differ from one another in the number, position, and configuration ...
T Iida, F C Chang, T Matsumoto, T Tamura
doaj +1 more source
For large-scale metabolomics, such as in cohort studies, normalization protocols using quality control (QC) samples have been established when using data from gas chromatography and liquid chromatography coupled to mass spectrometry.
Hiroyuki Yamamoto +8 more
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Alkenylbenzenes are potentially toxic (genotoxic and carcinogenic) compounds present in plants such as basil, tarragon, anise star and lemongrass. These plants are found in various edible consumer products, e.g., popularly used to flavour food.
Huynh N. P. Dang, Joselito P. Quirino
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