Results 1 to 10 of about 141,863 (280)

The Use of Polydialkylsiloxanes/Triflic Acid as Derivatization Agents in the Analysis of Sulfur-Containing Aromatics by “Soft”-Ionization Mass Spectrometry [PDF]

open access: goldMolecules, 2022
Polycyclic aromatic sulfur-containing compounds are widely distributed in oil, especially in its low-volatile and heavy fractions (resins, asphaltenes), and this dictates the need for their determination when reliable methods for sulfur removing ...
Zhanna Starkova   +9 more
doaj   +2 more sources

In-Needle Pre-Column Derivatization for Amino Acid Quantification (iPDAQ) Using HPLC

open access: yesMetabolites, 2022
Pre-column fluorescent derivatization has been used for the fast quantification of amino acids using high-performance liquid chromatography (HPLC) systems.
Yuki Soma   +11 more
doaj   +1 more source

Fluorimetric Analysis of Five Amino Acids in Chocolate: Development and Validation

open access: yesMolecules, 2021
Amino acids present ergogenic action, helping to increase, protect, and restore the muscular system of young athletes. Moreover, the encapsulation of five relevant amino acids in chocolate pellet form will appeal to them, facilitating their daily ...
Maria S. Synaridou   +5 more
doaj   +1 more source

Quantification of Intracellular Thiols by HPLC-Fluorescence Detection

open access: yesMolecules, 2021
Biothiols, such as cysteine and glutathione, play important roles in various intracellular reactions represented by the redox equilibrium against oxidative stress.
Hiroki Yamamoto   +3 more
doaj   +1 more source

Determination of Anthraquinone-Tagged Amines Using High-Performance Liquid Chromatography with Online UV Irradiation and Luminol Chemiluminescence Detection

open access: yesMolecules, 2023
Quinones are frequently used as derivatization reagents in HPLC analysis to improve detection sensitivity. In the present study, a simple, sensitive, and selective chemiluminescence (CL) derivatization strategy for biogenic amines, prior to their HPLC-CL
Naoya Kishikawa   +4 more
doaj   +1 more source

Metabolic Profiling and Quantitative Analysis of Cerebrospinal Fluid Using Gas Chromatography–Mass Spectrometry: Current Methods and Future Perspectives

open access: yesMolecules, 2021
Cerebrospinal fluid is a key biological fluid for the investigation of new potential biomarkers of central nervous system diseases. Gas chromatography coupled to mass-selective detectors can be used for this investigation at the stages of metabolic ...
Alisa Pautova   +2 more
doaj   +1 more source

An optimized analytical method for the simultaneous detection of iodoform, iodoacetic acid, and other trihalomethanes and haloacetic acids in drinking water [PDF]

open access: yes, 2013
An optimized method is presented using liquid-liquid extraction and derivatization for the extraction of iodoacetic acid (IAA) and other haloacetic acids (HAA9) and direct extraction of iodoform (IF) and other trihalomethanes (THM4) from drinking water ...
He, G   +6 more
core   +5 more sources

Development of Second-Tier Liquid Chromatography-Tandem Mass Spectrometry Analysis for Expanded Newborn Screening in Japan

open access: yesInternational Journal of Neonatal Screening, 2021
To minimize false-positive cases in newborn screening by tandem mass spectrometry in Japan, practical second-tier liquid chromatography-tandem mass spectrometry analyses have been developed using a multimode ODS column with a single set of mobile phases ...
Yosuke Shigematsu   +4 more
doaj   +1 more source

Towards a Non-Biased Formaldehyde Quantification in Leather: New Derivatization Conditions before HPLC Analysis of 2,4-Dinitrophenylhydrazine Derivatives

open access: yesMolecules, 2020
In leathers, formaldehyde is currently analyzed according to EN ISO 17226-1 standard, by reversed phase liquid chromatography after off-line precolumn derivatization with 2,4 dinitrophenylhydrazine (DNPH) in strong acidic conditions. We first demonstrate
Caroline Bourgeois   +3 more
doaj   +1 more source

Research Advances on Matrine

open access: yesFrontiers in Chemistry, 2022
Matrine is an alkaloid extracted from traditional Chinese herbs including Sophora flavescentis, Sophora alopecuroides, Sophora root, etc. It has the dual advantages of traditional Chinese herbs and chemotherapy drugs.
Xiao-Ying Sun   +20 more
doaj   +1 more source

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