Activation and Derivatization of Perfluoro(methyl Vinyl Ether) by a Rh(I) Germyl Complex
Treatment of the rhodium (I) germyl complex [Rh(GePh3)(PEt3)3] with perfluoro(methyl vinyl ether) [PMVE] resulted in CO and CF bond cleavage and decarbonylation reactions, to yield trans‐[Rh(CFCF2)(CO)(PEt3)2] and germylated species including fluorogermane FGePh3, and fluoroalkene CF(GePh3)CF2.
Soodeh Mollasalehi +2 more
wiley +1 more source
Comparative evaluation of phenyl isothiocyanate derivatization and "dilute-and-shoot" methods for HPLC-MS/MS-based targeted metabolomics analysis of amine-containing metabolites in plasma samples. [PDF]
Xu K +3 more
europepmc +1 more source
Cholesteryl Fatty Acid Esters and Free Cholesterol in Food of Animal Origin
Cholesterol occurs in free (bioavailable) and esterified (transport/storage) forms. Here, we present a method that allows both forms to be determined independently. Finally, the quantities of free and esterified cholesterol were determined in several meat, animal fat, and cheese samples.
Vanessa Hermann‐Ene +3 more
wiley +1 more source
A two-dimensional liquid chromatography method with optimized pretreatment for detection of guanidine compounds in animal liver and kidney. [PDF]
Ning KM +6 more
europepmc +1 more source
A comprehensive glycosylation study of diversely protected and activated d‐idopyranosyl and 6‐deoxy‐d‐ido‐heptopyranosyl donors using intra‐ and intermolecular coupling strategies is reported. Intramolecular aglycon delivery afforded 1,2‐cis‐β‐idopyranosides, while intermolecular glycosylation yielded chromatographically separable α‐ and β‐linked ...
Maude Cloutier +3 more
wiley +1 more source
Research and application of multi-component sterol determination methods in pre-prepared dishes. [PDF]
Ying Y +5 more
europepmc +1 more source
Recent Developments in Capillary and Microchip Electroseparations of Peptides (2023–mid 2025)
ABSTRACT This review presents a comprehensive overview of the developments and applications of high‐performance capillary and microchip electromigration methods (zone electrophoresis in a free solution or in sieving media, isotachophoresis, isoelectric focusing, affinity electrophoresis, electrokinetic chromatography, and electrochromatography) for ...
Václav Kašička
wiley +1 more source
Mass spectrometric profiling of microbial polysaccharides using laser desorption/ionization - time-of-flight (LDI-TOF) and liquid chromatography-mass spectrometry (LC-MS): a novel method for structural fingerprinting and derivatization. [PDF]
Dadovska L +3 more
europepmc +1 more source
Recent Advances in the Synthesis of 2-Substituted Oxetanes [PDF]
Bull, JA, Davis, O
core +1 more source
Determination of plasma ketone body following oximation-trimethylsily| derivatization using gas chromatography-mass spectrometry selected ion monitoring [PDF]
Hye‐Ran Yoon
openalex +1 more source

