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Electrospray Ionization Mass Spectrometry of Oligonucleotides
Current Protocols in Nucleic Acid Chemistry, 2008AbstractBecause of the high molecular weights and thermal lability of biomolecules such as nucleic acids and protein, they can be difficult to analyze by mass spectrometry. Such analyses require a “soft” ionization method that is capable of generating intact molecular ions.
Colette M. Castleberry +2 more
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Integration of electropreconcentration and electrospray ionization in a microchip
Journal of Chromatography A, 2018A microfluidic glass chip for performing sensitive mass spectrometry (MS) is developed by integrating nanochannel-based electropreconcentration with electrospray ionization (ESI). Cation analytes in acidic buffer conditions (∼pH 3) were preconcentrated at a micro-nano-microchannel junction where a positively charged polymer, polyE-323, is coated to ...
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Electrospray ionization source with a rear extractor
Journal of Mass Spectrometry, 2018AbstractA new electrospray source design is introduced by having an extractor electrode placed at 1 to 2 mm behind the emitter tip. The extractor was integrated into the sprayer body as a single device. An insulating tube was used to isolate the emitter from the extractor and to deliver the sheath gas for the electrospray.
Lee Chuin Chen +4 more
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Oxidation of peptides during electrospray ionization
Rapid Communications in Mass Spectrometry, 1993Abstract[M+H+16]+ ions were observed in the electrospray ionization mass spectra of several synthetic and maturally occurring peptides. Initial results have shown that the appearance of the modification is dependent on the field strength at the electrospray needle and the flow rate of the solution passing through the capillary.
Gert Talbo +2 more
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Electrospray ionization mass spectrometry of metalloporphyrins
Journal of Mass Spectrometry, 1998The magnesium, nickel, copper, zinc and vanadium metalloporphyrins from octaethylporphyrin, etioporphyrin I and tetraphenylporphyrin were characterized using electrospray ionization mass spectrometry (ESI-MS). The ion abundance of each of the porphyrins present in binary mixtures was monitored as a function of the porphyrin concentration and is ...
Patrick A. Limbach, Victor E. Vandell
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Generating Electrospray Ionization on Ballpoint Tips
Analytical Chemistry, 2016In this study, we report a simple and economical ballpoint electrospray ionization mass spectrometry (BP-ESI-MS) technique. This combines a small ballpoint tip with a syringe pump for the direct loading and ionization of various samples in different phases (including solution, semisolid, and solid) and allows for additional applications in surface ...
Yan Zhou +5 more
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Secondary Electrospray Ionization
2014This chapter details the technique called extractive electrospray ionization (EESI) and describes its state-of-the-art developmental, mechanical and experimental aspects and shows its most important applications. EESI is a sensitive, matrix-tolerant secondary electrospray ionization technique, which is in the focus of ongoing investigations.
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Special Feature on Electrospray Ionization
Journal of Mass Spectrometry, 2000Richard M. Caprioli, Graham Cooks
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Electrospray Laser Desorption Ionization
2019Electrospray laser desorption ionization (ELDI) combines the features of both electrospray ionization and laser desorption. It allows direct, sensitive, and rapid analyses of chemical compounds on the sample surfaces. Chemical and biological compounds dissolved in polar and nonpolar solvents can also be characterized directly by ELDI-mass spectrometry (
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Ion collection efficiency of ionization chambers in ultra‐high dose‐per‐pulse electron beams
Medical Physics, 2021Andreas Schüller, Daniela Poppinga
exaly