Results 71 to 80 of about 313,673 (292)

Thiol‐Modulation‐Induced Mesoporous Nanosheets with an Alloy/Intermetallic Heterophase for Efficient Electrochemical Ethylene Glycol‐Assisted Water Splitting

Advanced Functional Materials, EarlyView.
Sulfur‐capped mesoporous PtPbBi nanosheets (S‐PtPbBi MNSs) with an alloy/intermetallic compound heterophase and inhomogeneous tensile strain (≈3%) were synthesized by a thiol modification strategy, which exhibited excellent electrocatalytic performance for ethylene glycol oxidation reaction (EGOR).
Fukai Feng, Sumei Han, Chaoqun Ma, Xiao Ma, Gang Lin, Huaifang Zhang, Caihong He, Xinran Jiao, Xiangmin Meng, Wenbin Cao, Chongyi Ling, Lijie Zhu, Jing Xia, Qinbai Yun, Qipeng Lu   +14 more
wiley   +1 more source

A preliminary gas chromatography-mass spectrometry-based metabolomics study of rats ingested diazepam or clonazepam

Journal of Forensic Science and Medicine, 2020
Drug-facilitated sexual assault (DFSA) is a sexual act in which the victim is unable to give or rescind consent due to alcohol or drug intoxication, which involved the abuse of benzodiazepines around the world.
Shiyong Fang, Jianxia Chen, Xinhua Dai, Yuzi Zheng, Hao Wu, Yingqiang Fu, Jian Li, Yi Ye, Linchuan Liao   +8 more
doaj   +1 more source

Study of decomposition products by gas chromatography-mass spectrometry and ion chromatography-electrospray ionization-mass spectrometry in thermally decomposed lithium hexafluorophosphate-based lithium ion battery electrolytes

, 2015
In this work, the thermal decomposition of a lithium ion battery electrolyte (1 M LiPF6 in ethylene carbonate/ethyl methyl carbonate, 50/50 wt%) with a focus on the formation of organophosphates was systematically studied. The quantification of non-ionic
V. Kraft, Waldemar Weber, Martin Grützke, M. Winter, S. Nowak   +4 more
semanticscholar   +1 more source

Multifunctional Polyfluoride Ionogel‐Encapsulated Lithium Anodes for Durable and Safe Pouch Cells under Harsh Conditions

Advanced Functional Materials, EarlyView.
In this work, it is developed a multifunctional polyfluoride ionogel via in situ thermal polymerization to encapsulate lithium metal anodes, integrating flame‐retardant capability, hydrophobicity, dynamic self‐healing behavior, and high ionic conductivity.
Ting Li, Anjun Hu, Yuanjian Li, Borui Yang, Kun Li, Kai Chen, Jingyun Jiang, Fei Li, Zhi Wei Seh, Jian Wang, Jianping Long   +10 more
wiley   +1 more source

Applications of Solid-Phase Microextraction and Gas Chromatography/Mass Spectrometry (SPME-GC/MS) in the Study of Grape and Wine Volatile Compounds

Molecules, 2014
Volatile compounds are responsible for the wine “bouquet”, which is perceived by sniffing the headspace of a glass, and of the aroma component (palate-aroma) of the overall flavor, which is perceived on drinking.
A. Panighel, R. Flamini
semanticscholar   +1 more source

Covalent Adaptable Networks with Associative Siloxane Exchange Enabled by Amide‐Based Internal Catalysis: Designing for Reprocessability and Extrudability by Increasing the Cross‐Link Density

Advanced Functional Materials, EarlyView.
Internally catalyzed siloxane dynamic chemistry is demonstrated resulting from amides covalently linked through alkyl chains to siloxanes. The alkyl length in the siloxane‐containing monomer tunes the network cross‐link density. Siloxane exchange dynamics are faster with increasing cross‐link density, because associative exchange is second order in ...
Nathan S. Purwanto, Tong Wang, Xiaoyang Liu, Linda J. Broadbelt, Tapas Debsharma, John M. Torkelson   +5 more
wiley   +1 more source

Determination of ifosfamide by gas chromatography—mass spectrometry

Analytica Chimica Acta, 1991
Ifosfamide, an oxazaphosphorine, is thermally stable during elution in gas chromatography (GC) at temperatures above 200 °C, in contrast to its structural isomer cyclophosphamide. Both 2.65-µm and 0.32-µm OV-1 columns were efficient for GC of ifosfamide without derivatization.
Hilde A. J. Lambrechts, Allan T. van Oosterom, PA Piet Leclercq, Greet G. O. Pattyn, Karel Van Cauwenberghe, Ernst A. de Bruijn, Eric O.O. Gheuens   +6 more
openaire   +2 more sources

Metal‐Organic Nanosheet Gels: Hierarchically Porous Materials for Selective Loading and Differential Release

Advanced Functional Materials, EarlyView.
A suspension of metal‐organic nanosheets was centrifuged to form self‐healing gels with a hierarchically porous structure. The prepared gels were used to selectively capture small molecules from solutions and differentially release them based on their size and charge. Abstract Metal‐organic nanosheets (MONs) are intrinsically porous 2D materials with a
Jiangtian Tan, Jonathan A. Foster
wiley   +1 more source

Highly Sensitive Electrochemical Biosensor Based on Hairy Particles with Controllable High Enzyme Loading and Activity

Advanced Functional Materials, EarlyView.
For the first time, a highly sensitive electrochemical biosensor based on SiO2‐based hairy particles with a grafted PDMAEMA polymer brush containing a quantifiable and large amount of immobilized Laccase is reported. The fabricated biosensor exhibits a sensitivity of 0.14 A·m⁻¹, a limit of detection (LOD) of 0.1 µm, and a detection range of 0.3–750 µm,
Pavel Milkin, Anila Antony, Hongtao Cai, Antonia Debevc, Ceyda Topal, Anne Linhardt, Alla Synytska, Leonid Ionov   +7 more
wiley   +1 more source

Isolation and characterization of a novel uronic acid-containing acidic glycosphingolipid from the ascidian Halocynthia roretzi

Journal of Lipid Research, 2007
A novel uronic acid-containing glycosphingolipid (UGL-1) was isolated from the ascidian Halocynthia roretzi. UGL-1 was prepared from chloroform-methanol extracts and purified by the use of successive column chromatography on DEAE-Sephadex, Florisil, and ...
Masahiro Ito, Yuki Matsumuro, So Yamada, Tomonori Kitamura, Saki Itonori, Mutsumi Sugita   +5 more
doaj   +1 more source