Results 191 to 200 of about 500,833 (298)

Effect of Reaction Time and Temperature on the Impurity Profile of Amphetamine in the Leuckart Method

open access: yesDrug Testing and Analysis, EarlyView.
This study investigates the effect of the reaction temperature (step 1) and reaction time (step 1 and 2) on the conversion efficiency and impurity profile of amphetamine synthesized via the Leuckart method. Conversion efficiency and impurity profile were assessed using gas chromatography–flame ionization detection (GC–FID) and GC–mass spectrometry (GC ...
Maartje C. M. Verhoeven   +7 more
wiley   +1 more source

Effect of dislocation slip on in-situ tensile fracture of vanadium alloys after helium/self-ion irradiation. [PDF]

open access: yesSci Technol Adv Mater
Zhang Q   +6 more
europepmc   +1 more source

Influence of Different Washing Hair Procedures in the Quantitative Determination of THC and THCCOOH

open access: yesDrug Testing and Analysis, EarlyView.
Different hair decontamination protocols significantly affect THC quantification, with marked analyte loss—particularly after aqueous‐organic washing—whereas THCCOOH remains stable. These findings highlight the risk of misinterpretation and the need for standardized washing procedures in hair analysis.
Valentina Martini   +8 more
wiley   +1 more source

Identification and Characterization of the Designer Opioid N‐Pyrrolidino Fluetonitazene in Nasal Spray

open access: yesDrug Testing and Analysis, EarlyView.
N‐Pyrrolidino fluetonitazene, a synthetic opioid, was identified and characterized in a nasal spray using GC‐MS, LC‐QTOF‐MS, NMR and FT‐IR. ABSTRACT Detection of drugs in non‐biological samples serves as a fundamental basis for identifying emerging trends in the field of new psychoactive substances and provides valuable information for optimizing ...
Fabian Picht   +4 more
wiley   +1 more source

Defect Engineering and Effect of Vacancy Concentration on the Electrochemical Performance of V‐Based MXenes

open access: yesENERGY &ENVIRONMENTAL MATERIALS, EarlyView.
Using a top‐down defect engineering approach, controllable vacancy concentrations are introduced into V‐based MXenes by rationally designing the precursor MAX phase, aiming to investigate the effect of vacancy concentration on the electrochemical performance.
Leiqiang Qin   +7 more
wiley   +1 more source

Nanofiber PVA‐Based Membranes Incorporating Functionalized Spanish Broom Derivatives for Sustainable Water Purification

open access: yesENERGY &ENVIRONMENTAL MATERIALS, EarlyView.
This study investigates Spanish broom (Spartium junceum) as a renewable source for electrospun composite membranes in sustainable water purification. MCC and biochar were functionalized with eco‐friendly precursors and nanomaterials (i.e., HNT, β‐CDs) to develop hybrid PVA nanofiber composites.
Giulia Rando   +7 more
wiley   +1 more source

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