Results 131 to 140 of about 131,872 (335)

Heterogeneously Catalyzed Cascade Oxidative Coupling/Dearomative Spirocyclization of Diarylamines: Facile Access to Spiroacridines

open access: yesAdvanced Synthesis &Catalysis, EarlyView.
Abstract Spirocyclic compounds, particularly spirocyclohexadienones, are important in pharmaceuticals due to their biological activity. In this study, we develop a catalytic cascade oxidative spirocyclization of diarylamines for the rapid access to highly functionalized spirocyclohexadienones. Using commercially available recyclable heterogeneous metal
Kenji Matsumoto   +7 more
wiley   +1 more source

EKSTRAKSI MINYAK DAN RESIN NYAMPLUNG DENGAN CAMPURAN PELARUT HEKSAN-ETANOL

open access: yesJurnal Teknologi Industri Pertanian, 2017
Calophyllum seeds are potential to be used as raw material for vegetable oil production due to their high oil content (75.1% db). In addition, Calophyllum seeds contain resin consistingbeneficial phenolic compounds for health.
Ika Amalia Kartika   +4 more
doaj  

Asymmetric synthesis of highly substituted spiro[2H‐pyrrole‐2,3‐succinimide] derivatives by copper‐catalyzed post‐Ugi reactions

open access: yesAdvanced Synthesis &Catalysis, Accepted Article.
Herein we present a novel one‐por methodology for the synthesis of enantioenriched 2H‐pyrrolespirosuccinimides by copper‐catalyzed reactions on Ugi adducts derived from enantiopure α‐alkylbenzyl amines through a chirality transfer process. We have proposed a mechanism supported by density functional theory (DFT) calculations, where a hydrogen radical ...
Maria Garcia Valverde   +3 more
wiley   +1 more source

Development of Photo‐Biocatalytic Redox System for Asymmetric Synthesis of Optically Active Amines Using Blue Light and Transaminases. A Case Study Toward Mavacamten

open access: yesAdvanced Synthesis &Catalysis, EarlyView.
Abstract α‐Chiral amines are versatile building blocks for the asymmetric synthesis of optically pure high‐added‐value chemicals, including pharmaceuticals, agrochemicals, and natural products. Herein, we report a one‐pot, two‐step sequential deracemization of racemic sec‐alcohols to optically enriched primary amines throught a photo‐biocatalytic ...
Natalia Antos   +5 more
wiley   +1 more source

Modular Synthesis of 2,3,4,6‐Tetrasubstituted Thieno[2,3‐c]furans Based on Formal [3+2] Cycloaddition Utilizing [1,2]‐Phospha‐Brook Rearrangement / Brønsted Base‐Mediated Cyclization Strategy

open access: yesAdvanced Synthesis &Catalysis, EarlyView.
Abstract A modular synthesis of 2,3,4,6‐tetrasubstituted thieno[2,3‐c]furans, which employs a formal [3+2] cycloaddition utilizing the [1,2]‐phospha‐Brook rearrangement and a subsequent Brønsted base‐mediated cyclization, has been established, providing an efficient access to a wide range of densely functionalized thieno[2,3‐c]furans that are otherwise
Azusa Kondoh   +2 more
wiley   +1 more source

Optimized Pt Loaded Cerium Tungstate Electrochemical Sensor for Rapid Response and Recovery NO2 Detection

open access: yesAdvanced Sensor Research, EarlyView.
Pt/Ce2(WO4)3, synthesized via simple calcination and hydrothermal methods, serves as a promising electrochemical gas sensor for detecting nitrogen dioxide (NO2). This study investigates the structural characteristics of the sensor. The sensor with 0.5 wt.% Pt loading exhibits the optimal sensing performance, demonstrating high sensitivity and ...
Jiaxin Li   +3 more
wiley   +1 more source

Impact of edaphoclimatic conditions and crop season on olive oil's fatty acids

open access: yesAgronomy Journal, Volume 114, Issue 6, Page 3118-3128, November/December 2022., 2022
Abstract The olive tree (Olea europaea L.) fruit oil attracts widespread interest because of its high content of monounsaturated fatty acids. However, a neglected area in the field is the edaphoclimatic factors impact, which is poorly understood. Bearing this in mind, the purpose of this investigation was to evaluate the impact of the edaphoclimatic ...
Touria Lechhab   +5 more
wiley   +1 more source

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