Results 91 to 100 of about 435,222 (363)

Chemical and toxicological analysis of zolpidem

open access: yesRUDN Journal of Medicine, 2009
Methods for measuring zolpidem are suggested: thin-layer chromatography, high-pressure liquid chromatography, ultrtaviolet spectrophotometry, gas chromatography with mass selective detector can be used for identification zolpidem in chemical ...
Y A Khomov   +3 more
doaj  

High Pressure Liquid Chromatography of Zearalenone in Cereals

open access: yesJournal of AOAC INTERNATIONAL, 1978
Abstract A high pressure liquid chromatographic method has been developed for determining zearalenone in cereals. The sample is extracted with phosphoric acid and chloroform. The extract is cleaned up by washing on a silica gel column with benzene-hexane or cyclohexaneethylene dichloride-ethyl ether and eluting with chloroform, and ...
Tord E Möller, Egon Josefsson
openaire   +3 more sources

Qualitative and quantitative phytochemical analysis of different extracts from Thymus algeriensis aerial parts [PDF]

open access: yes, 2018
This study was performed to evaluate the metabolite recovery from different extraction methods applied to Thymus algeriensis aerial parts. A high-performance liquid chromatographic method using photodiode array detector with gradient elution has been ...
Benayache, Fadila   +10 more
core   +2 more sources

Tunable Thermoshrinkable Hydrogels for 4D Fabrication of Cell‐Seeded Channels

open access: yesAdvanced Functional Materials, EarlyView.
A thermoresponsive polymer with methacrylate groups for photo‐cross‐linking, based on polyethylene glycol, N‐isopropylacrylamide, and 2‐hydroxyethyl acrylate is synthetized to yield hydrogels that shrink upon temperature increase. The new polymer enables the fabrication of cell‐laden perfusable channels with diameters below 200 µm by combining ...
Greta Di Marco   +12 more
wiley   +1 more source

The separation of sterol intermediates in cholesterol biosynthesis by high pressure liquid chromatography

open access: yesJournal of Lipid Research, 1980
A three-step procedure has been developed for the separation of complex mixtures of sterol intermediates in cholesterol biosynthesis. The method has been applied to the separation of sterol intermediates formed from [14C]mevalonate by normal rat ...
E Hansbury, T J Scallen
doaj  

Investigating the Structure–Function Relationships of Fluorinated Interfaces for PFAS Capture and Electrochemically‐Mediated Release

open access: yesAdvanced Functional Materials, EarlyView.
This study explores the use of fluorinated copolymers with varying fluorophilic side chain lengths to enhance PFAS affinity. The integration of electrochemical techniques demonstrates enhanced adsorbent regeneration, with molecular dynamics simulations providing insight into the molecular‐level interactions involved.
Anaira Román Santiago   +7 more
wiley   +1 more source

Characterization and toxicity evaluation of degradation products of febantel

open access: yesFuture Journal of Pharmaceutical Sciences, 2020
Background The aim of the present work was to determine potential toxicity of degradation products of febantel generated under different stress conditions mentioned in guideline Q1A (R2) laid down by International Council for Harmonization (ICH).
Anand A. Mahajan   +4 more
doaj   +1 more source

Deciphering a New Electrolyte Formulation for Intelligent Modulation of Thermal Runaway to Improve the Safety of Lithium‐Ion Batteries

open access: yesAdvanced Functional Materials, EarlyView.
Diels‐Alder clicks chemistry addresses thermal runaway in lithium‐ion batteries. A thermoresponsive electrolyte with lithium salt in vinylene carbonate (VC) and 2,5‐dimethylfuran (DMFu) operates at room temperature but undergoes Diels‐Alder reactions at high temperatures, enabling a two‐step safety mechanism: a warning phase at ≈100 °C and complete ...
Arnab Ghosh   +9 more
wiley   +1 more source

Machine Learning‐Enabled Polymer Discovery for Enhanced Pulmonary siRNA Delivery

open access: yesAdvanced Functional Materials, EarlyView.
This study provides an efficient approach to train a machine learning model by merging heterogeneous literature data to predict suitable polymers for siRNA delivery. Without the need for extensive laboratory synthesis, the machine learning enabled a virtual screening and successfully predicted a polymer that is validated for effective gene silencing in
Felix Sieber‐Schäfer   +10 more
wiley   +1 more source

Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol.

open access: yesJournal of Lipid Research, 1979
Conditions have been described which permit the rapid (approximately 3.5 hr) column chromatographic separation of the acetate derivatives of a number of C27 sterol precursors of cholesterol differing only in the number and position of double bonds in the
J R Thowsen, G J Schroepfer, Jr
doaj  

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