Results 41 to 50 of about 509,811 (262)

Possibilidades e limitações no uso da temperatura em cromatografia líquida de fase reversa Possibilities and limitations of using temperature in reversed phase liquid chromatography

open access: yesQuímica Nova, 2010
High-temperature liquid chromatography (HTLC) is a technique that presents a series of advantages in liquid phase separations, such as: reduced analysis time, reduced pressure drop, reduced asymmetry factors, modified retentions, controlled selectivities,
Endler Marcel Borges   +2 more
doaj   +1 more source

Chemical and toxicological analysis of zolpidem

open access: yesRUDN Journal of Medicine, 2009
Methods for measuring zolpidem are suggested: thin-layer chromatography, high-pressure liquid chromatography, ultrtaviolet spectrophotometry, gas chromatography with mass selective detector can be used for identification zolpidem in chemical ...
Y A Khomov   +3 more
doaj  

High Pressure Liquid Chromatography of Zearalenone in Cereals

open access: yesJournal of AOAC INTERNATIONAL, 1978
Abstract A high pressure liquid chromatographic method has been developed for determining zearalenone in cereals. The sample is extracted with phosphoric acid and chloroform. The extract is cleaned up by washing on a silica gel column with benzene-hexane or cyclohexaneethylene dichloride-ethyl ether and eluting with chloroform, and ...
Tord E Möller, Egon Josefsson
openaire   +3 more sources

High-Pressure Liquid Chromatography of Caffeine in Coffee

open access: yesJournal of AOAC INTERNATIONAL, 1976
Abstract A new method is described for the determination of caffeine in coffee, based on high-pressure liquid chromatography. The caffeine is extracted from the sample with water and/or methylene chloride, and then separated from interfering materials by passing an aliquot of the extract through a high-pressure column containing ...
Bryan L Madison   +2 more
openaire   +2 more sources

Determination of captopril by hplctandem mass spectrometry: application in a bioequivalence study [PDF]

open access: yesRevista Brasileira em Promoção da Saúde, 2012
Objective: To assess three different captopril tablet formulations of 25mg for their bioavailability (Capoten® as the reference formulation and Captopril from FURP and Farmanguinhos as the test formulations) in 24 healthy volunteers of both sexes ...
Aline Kércia Alves Soares   +4 more
doaj  

Clinical application of blood concentration monitoring of active metabolite of oxcarbazepine in childhood focal epilepsy

open access: yesChinese Journal of Contemporary Neurology and Neurosurgery, 2018
Objective To investigate the value of blood concentration monitoring of 10-monohydroxy carbamazepine (MHD), the active metabolite of oxcarbazepine (OXC), in the treatment ofchildhood focal epilepsy.
Pei-yuan ZHANG   +4 more
doaj   +1 more source

Resolution of desmosterol, cholesterol, and other sterol intermediates by reverse-phase high-pressure liquid chromatography.

open access: yesJournal of Lipid Research, 1978
A highly efficient technique has been developed for the resolution of several sterols that are intermediates in the biosynthesis of cholesterol and that differ only by one carbon-carbon double bond or by one methyl group. The technique described utilizes
E Hansbury, T J Scallen
doaj   +1 more source

Characterization and toxicity evaluation of degradation products of febantel

open access: yesFuture Journal of Pharmaceutical Sciences, 2020
Background The aim of the present work was to determine potential toxicity of degradation products of febantel generated under different stress conditions mentioned in guideline Q1A (R2) laid down by International Council for Harmonization (ICH).
Anand A. Mahajan   +4 more
doaj   +1 more source

The development and validation of HPLC-DMD method for intermediate products impurities determination of morpholinium 2-((4-(2-methoxyphenyl)-5-(pyridine-4-yl)-4H-1,2,4-triazole-3-yl)thio)acetate in bulk drug

open access: yesZaporožskij Medicinskij Žurnal, 2017
Purpose. A development and validation of new sensitive, high efficient and selective HPLC determination method of intermediates technological contaminations in bulk drug of morpholin-4-ium 2-((4-(2-methoxyphenyl)-5-(pyridine-4-yl)-4H-1,2,4-triazole-3-yl ...
B. O. Varynskyi, A. G. Kaplaushenko
doaj   +1 more source

Comparison of Capillary Zone Electrophoresis with High-pressure Liquid Chromatography in the Evaluation of Hemoglobinopathies [PDF]

open access: yesTurk J Haematol, 2023
Çakır Madenci Ö   +4 more
europepmc   +1 more source

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