Pitfall in the high-throughput quantification of whole blood cyclosporin A using liquid chromatography-tandem mass spectrometry [PDF]
In a growing number of laboratories the technique of liquid chromatography-tandem mass spectrometry is used for the quantification of cyclosporin A in whole blood, employing cyclosporin D as the internal standard. Cyclosporin A is extensively metabolized
Michael Vogeser +3 more
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High pressure liquid chromatography solvent systems for studies of bile acid biosynthesis.
Reversed phase high pressure liquid chromatography (HPLC) solvent systems have been developed for the separation of intermediates in the formation of bile acids and bile acid conjugates from cholesterol.
K Prydz, B F Kase, J I Pedersen
doaj +1 more source
Ultra-High-Pressure Liquid Chromatography ☆ [PDF]
One decade has passed since the introduction of commercial ultra-high-pressure liquid chromatography (UHPLC) technology and columns packed with sub-2-μm particles, which has led to significant improvements in separation efficiency and sample throughput. This article outlines fundamental and practical aspects of UHPLC.
Eeltink, Sebastiaan, De Vos, Jelle
openaire +2 more sources
Aim: Quantification of urinary ortho-cresol (OC) by high pressure liquid chromatography coupled with photodiode array detector. Materials and Methods: Includes acid hydrolysis of urine, liquid–liquid extraction, and chromatography quantification of ...
Anupa Yadav +2 more
doaj +1 more source
Enricher for Fraction of High-Pressure Liquid Chromatography [PDF]
A device is developed for concentrating a dilute solution without losing the components with boiling points slightly higher than the solvent. The device consists of an evaporator, receptor, and approximately 100 capillaries. A dilute solution is introduced into the evaporator and heated at a lower temperature than the boiling point of the solvent with ...
Tadao, Ogawa +2 more
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Validation of a chromatographic method to routine analysis of trans-resveratrol and quercetin in red wines [PDF]
: The objective of this work was to validate a fast method with low-solvent use, for the analysis of trans-resveratrol and quercetin in red wines. The wines were prepared, using a classical method, from the grape (Vitis vinifera) cultivars Cabernet Franc,
Letícia Flores da Silva +4 more
doaj +1 more source
Integrated Nano Liquid Chromatography System On-a-Chip [PDF]
Integrated liquid chromatography (LC) chips are valued because of their significant advantages over conventional systems. However, they are very challenging to build due to the high complexity of LC systems and the need for high-level integration of many
He, Qing
core +1 more source
Analysis of ochratoxin A in pig tissues using high pressure liquid chromatography (HPLC) and liquid chromatography tandem mass spectrometry (LC/MS/MS) as confirmative methods [PDF]
Two different analytical methods for the determination and confirmation of ochratoxin A (OTA) in blood serum, kidney and liver of pigs have been compared. Sample clean-up was based on liquid-liquid phase extraction.
Milićević Dragan R. +4 more
doaj +1 more source
Liquid chromatography-tandem mass spectrometry - Application in the clinical laboratory [PDF]
This review provides a concise survey of liquid chromatography tandem mass spectrometry (LCTMS) as an emerging technology in clinical chemistry. The combination of two mass spectrometers with an interposed collision cell characterizes LCTMS as an ...
Michael Vogeser, Vogeser, Michael
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Numerical Simulation of Fluid Dynamics in a Monolithic Column
As for the measurement of polycyclic aromatic hydrocarbons (PAHs), ultra-performance liquid chromatography (UPLC) is used for PAH identification and densitometry.
Kazuhiro Yamamoto, Yuuta Tajima
doaj +1 more source

