Plasma L-ergothioneine measurement by high-performance liquid chromatography and capillary electrophoresis after a pre-column derivatization with 5-iodoacetamidofluorescein (5-IAF) and fluorescence detection [PDF]
, 2013 Two sensitive and reproducible capillary electrophoresis and high-performance liquid chromatography-fluorescence procedures were established for quantitative determination of L-egothioneine in plasma.
Carru, Ciriaco +7 more
core +2 more sources
On the Determination of Uncertainty and Limit of Detection in Label-Free Biosensors
Sensors, 2018 A significant amount of noteworthy articles reviewing different label-free biosensors are being published in the last years. Most of the times, the comparison among the different biosensors is limited by the procedure used of calculating the limit of ...
Álvaro Lavín +8 more
doaj +1 more source
The phylogenetic effective sample size and jumps
, 2018 The phylogenetic effective sample size is a parameter that has as its goal the quantification of the amount of independent signal in a phylogenetically correlated sample. It was studied for Brownian motion and Ornstein-Uhlenbeck models of trait evolution.
Bartoszek, Krzysztof
core +1 more source
Rate-independent evolution of sets [PDF]
, 2019 The goal of this work is to analyze a model for the rate-independent evolution of sets with finite perimeter. The evolution of the admissible sets is driven by that of a given time-dependent set, which has to include the admissible sets and hence is to ...
Rossi, Riccarda +2 more
core +3 more sources
Molecules, 2019 The crystal structure of the new polymorphic form of 3-aminoflavone (3-AF) has been determined by single crystal X-ray diffraction. This report presents results of fluorimetric studies on 3-AF in methanol and aquatic solvents.
Wojciech Pająk +6 more
doaj +1 more source
Quantification of joint mobility limitation in adult type 1 diabetes
Frontiers in Endocrinology, 2023 Aims Diabetic cheiroarthropathies limit hand mobility due to fibrosis and could be markers of a global profibrotic trajectory. Heterogeneity in definitions and lack of a method to measure it complicate studying associations with organ involvement and treatment outcomes.
Sanat Phatak +12 more
openaire +3 more sources
New Method for Simultaneous Determination of Microcystins and Cylindrospermopsin in Vegetable Matrices by SPE-UPLC-MS/MS [PDF]
, 2018 Cyanotoxins are a large group of noxious metabolites with different chemical structure and mechanisms of action, with a worldwide distribution, producing effects in animals, humans, and crop plants.
Cameán Fernández, Ana María +7 more
core +1 more source
Hittite Journal of Science and Engineering, 2016 This study represents a high performance liquid chromatography HPLC method for the detection of 5-hydroxymethylfurfural in pestil, köme, jam and pekmez samples.
Cemalettin Baltacı, Zeynep Akşit
doaj +1 more source
Development and validation of a GC-MS method for the detection and quantification of clotiapine in blood and urine specimens and application to a postmortem case [PDF]
, 2015 INTRODUCTION: Clotiapine is an atypical antipsychotic of the dibenzothiazepine class introduced in a few European countries since 1970, efficient in treatment-resistant schizophrenic patients.
Busardo', FRANCESCO PAOLO +5 more
core +5 more sources
Revista de Ciências Farmacêuticas Básica e Aplicada, 2021 Objective. The aim of this study was the development and validation of an UV-Vis spectrophotometric method for the quantification of oclacitinib in commercial capsule formulation since pharmacopeias have not yet provided an official monograph for this ...
Danilo R. O. Momade +7 more
doaj +2 more sources