Results 31 to 40 of about 9,099 (177)

Micro‐QuEChERS Extraction for Broad‐Spectrum LC‐QQQ‐MS Quantification of Nitazene Analogs in Plasma: A Validated Method With Casework Application

Drug Testing and Analysis, EarlyView.
Micro‐QuEChERS sample preparation coupled to LC‐QQQ‐MS enabled sensitive quantification of nitazene analogs in 100 μL of plasma. The validated method provided low detection limits and was successfully applied to an authentic intoxication case involving N‐pyrrolidino protonitazene, supporting clinical and forensic toxicology workflows.
Karla A. O. Souza, Náthaly C. B. F. Santos, Rafael Lanaro, Sara E. Walton, Alex J. Krotulski, Barry K. Logan, Mauricio Yonamine, Jose Luiz Costa   +7 more
wiley   +1 more source

Sample treatment platform for automated integration of microextraction techniques and liquid chromatography analysis

HardwareX, 2019
Sample preparation performance influences the quality of every chemical analysis. Since it is the most labor-intensive stage in the nearly all-analytical protocols, sample preparation automation would be desirable, to increase the analytical throughput ...
Deyber Arley Vargas Medina, Luís Felipe Rodriguez Cabal, Fernando Mauro Lanças, Álvaro José Santos-Neto   +3 more
doaj   +1 more source

Cyclodextrins as Chiral Selectors in Capillary Electrophoresis—Recent Developments in Understanding Analyte Complexation and Applications in Pharmaceutical Analysis

ELECTROPHORESIS, EarlyView.
Cyclodextrins are the most often applied chiral selectors in CE enantioseparations. In combination with NMR spectroscopy and molecular modeling, studies for an understanding of chiral recognition underlying enantioseparations have been performed.
Gerhard K. E. Scriba
wiley   +1 more source

Stir Bar Sorptive Extraction - New Approach for the Determination of Some Beer Flavours.

Kvasný průmysl, 2008
For the determination of beer flavours well-established methods require sample preparation steps such as liquid/liquid extraction, solid phase extraction or distillation techniques. During the past years the microextraction procedures become popular e. g.
Tomáš HORÁK, Jiří ČULÍK, Marie JURKOVÁ, Pavel ČEJKA, Vladimír KELLNER   +4 more
doaj   +1 more source

Monitoring and Mitigation Strategies for Hazardous Compounds in Chinese Rice Wine (Huangjiu): A Comprehensive Review

Food Safety and Health, EarlyView.
This review elucidates the formation pathways and detection technologies for ethyl carbamate, biogenic amines, and higher alcohols in Huangjiu. It concludes that integrated control frameworks are essential to decouple safety risks from the metabolic processes responsible for flavor development.
Lulu Liu, Zhiqiang Kong, Lin Li, Yifan Zhang, Bei Fan, Minmin Li   +5 more
wiley   +1 more source

Biological activities and bioactive constituents of Flammulina velutipes: An updated systematic review

Journal of the Science of Food and Agriculture, EarlyView.
Abstract Flammulina velutipes (enokitake) is an edible mushroom recognized for both its nutritional and medicinal properties. It exhibits a broad spectrum of biological activities, including antioxidant, anti‐inflammatory, antitumor, immunomodulatory, and gut microbiota‐regulating effects.
Rıdvan Özgen, Didem Şöhretoğlu, Ayşe Kuruüzüm‐Uz   +2 more
wiley   +1 more source

Valorization of Zingiber officinale Roscoe leaf biomass: phytotoxic potential and chemical profiling toward sustainable weed management

Journal of the Science of Food and Agriculture, EarlyView.
Abstract BACKGROUND Zingiber officinale Roscoe is widely cultivated as a spice and functional food, generating substantial amounts of aerial biomass that is commonly discarded after harvest. Within a circular‐economy framework, this study investigated the phytotoxic potential of Z.
Sara Vitalini, Orlando Innaurato, Shadab Faramarzi, Alessandro Palmioli, Stefania Garzoli, Valentina Vaglia, Cristina Airoldi, Marcello Iriti   +7 more
wiley   +1 more source

Applications of Microextraction Technology for the Analysis of Alcoholic Beverages Quality: Current Perspectives and Future Directions

Foods
Alcoholic beverages are loved by the majority of consumers because of their diverse characteristics and rich nutritional value; thus, ensuring their quality is necessary for maintaining the rapid development of the alcoholic beverage industry.
Yue Qiu, Qi Deng, Yongqing Zhang, Baoguo Sun, Wenxian Li, Wei Dong, Xiaotao Sun   +6 more
doaj   +1 more source

The recent developments in dispersive liquid–liquid microextraction for preconcentration and determination of inorganic analytes

Journal of Saudi Chemical Society, 2014
Recently, increasing interest on the use of dispersive liquid–liquid microextraction (DLLME) developed in 2006 by Rezaee has been found in the field of separation science.
H.M. Al-Saidi, Adel A.A. Emara
doaj   +1 more source

Application of Dispersive Liquid-Liquid Microextraction in Forensic Toxicological Analysis [PDF]

Fayixue Zazhi, 2019
Currently, the main sample pretreatment methods for forensic toxic analysis are liquid-liquid extraction （LLE） and solid-phase extraction （SPE）. As a simple, convenient, and low-cost LLE method, dispersion liquid-liquid microextraction （DLLME） has high ...
YANG Yu, ZHANG Yun-feng, LI Xin-tong，et al.
doaj   +1 more source