Results 141 to 150 of about 49,096 (297)

Structural Profiling of Lipid Nanoparticles at Sub‐10 nm Resolution via AF4 Coupled Online to SAXS and SANS

open access: yesSmall Methods, EarlyView.
Dilution‐controlled AF4 coupled with SAXS and, for the first time, SANS enables high‐resolution characterization of non‐spherical lipid nanoparticles. Enhanced scattering contrast and D2O‐based measurements resolve particle features down to ∼5 nm and reveal shape distributions.
Eva Bittrich   +12 more
wiley   +1 more source

Low‐Dose Electron Total Scattering Analysis Resolves Non‐Crystalline Phase Separation in Polymer Semiconductors and Device Multilayers

open access: yesSmall Methods, EarlyView.
The performance of polymer blend semiconductors is governed by both the degree of phase separation and crystallization, but these two aspects have remained unresolved. We report methods for mapping amorphous‐amorphous as well as amorphous‐crystalline phase separation in polyfluorene‐based polymer blends using spatially resolved nanobeam electron total ...
Sang T. Pham   +2 more
wiley   +1 more source

Recycling End‐of‐Life Solid Oxide Cell Interconnect Assemblies into Commercial‐Grade AISI 304 Stainless Steels

open access: yessteel research international, EarlyView.
This study validates a recycling pathway for converting interconnect assemblies from end‐of‐life SOC stacks into commercial‐grade AISI 304 steels. Using scrap‐based steelmaking operations, austenitic cast steels with <4.0% δ‐ferrite are successfully produced.
Jeraldine Lastam   +7 more
wiley   +1 more source

Crystal Structures and Magnetic Properties of Coordination Polymer Complexes of Metal Ions With Kojic Acid Ligands

open access: yesZeitschrift für anorganische und allgemeine Chemie, EarlyView.
One‐dimensional coordination polymers of Cu(II) and Co(II) with kojic acid show distinct chain connectivities revealed by X ray crystallography and exhibit extremely weak magnetic interactions, as supported by magnetic measurements and molecular orbital calculations. The crystal structures and magnetic properties of coordination complexes [Cu(C6H5O4)2]
Wataru Fujita, Tomoko Yamaguchi
wiley   +1 more source

Approximate resolution convolution function for fitting a dispersion gap measured on a triple‐axis spectrometer

open access: yesJournal of Applied Crystallography, EarlyView.
An analytical convoluted gap function is presented for fitting either a linear or a quadratic dispersion gap in a constant‐Q cut measured with a focused triple‐axis spectrometer. It outperforms previous methods of fitting a gap, without requiring a full resolution convolution.We present an analytical convoluted gap function for fitting dispersion gaps ...
Emma Y. Lenander   +3 more
wiley   +1 more source

Solid state neutron dosimeter for space applications [PDF]

open access: yes
Personnel engaged in space flight are exposed to significant flux of high energy neutrons arising from both primary and secondary sources of ionizing radiation.
Entine, Gerald   +2 more
core   +1 more source

Integrating simultaneous interfacial shear rheology with neutron reflectometry for structural and dynamic analysis of fluid interfacial systems

open access: yesJournal of Applied Crystallography, EarlyView.
We present a new setup at the FIGARO horizontal neutron reflectometer enabling simultaneous measurement of the structural and mechanical properties of liquid interfaces, combining neutron reflectometry with interfacial shear rheology.The study of the structure and mechanical properties of complex fluid interfaces has attracted growing interest in ...
Pablo Sánchez-Puga   +5 more
wiley   +1 more source

mcstas_gisans: combining ray tracing with the distorted‐wave Born approximation using McStas and BornAgain for virtual GISANS experiments

open access: yesJournal of Applied Crystallography, EarlyView.
mcstas_gisans is a Python‐based framework that enables simulation of grazing‐incidence small‐angle neutron scattering experiments by integrating McStas and BornAgain into a single workflow.The mcstas_gisans framework is a collection of Python scripts and modules to facilitate the simulation of grazing‐incidence small‐angle neutron scattering (GISANS ...
Milán Klausz   +8 more
wiley   +1 more source

Magnetic structure in the two‐dimensional van der Waals ferromagnet Fe3GaTe2

open access: yesJournal of Applied Crystallography, EarlyView.
High‐quality single crystals of Fe3GaTe2 were grown using the chemical vapour transport method, allowing for a precise determination of their crystal and magnetic structures. A shortening of the Fei–Fei distance enhances the Fe–Fe exchange interaction, providing a microscopic origin for its higher Curie temperature compared with Fe3GeTe2.High‐quality ...
Po-Chun Chang   +7 more
wiley   +1 more source

Computational methods for automated center determination in electron diffraction patterns

open access: yesJournal of Applied Crystallography, EarlyView.
This study evaluates and compares automated methods for center detection in 2D diffractograms. The methods have been implemented in EDIFF, an open‐source user‐friendly Python package for the processing of electron diffraction patterns.Accurate center detection in electron diffraction patterns is critical for all subsequent processing of experimental ...
Pavlina Sikorova   +3 more
wiley   +1 more source

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