Results 211 to 220 of about 468,653 (298)

Dual Lewis Acid Promoted/Visible Light Driven Preparation of Aryl Diazenyl Oxazoles from Isocyanoacetamides and Arylazo Sulfones

open access: yesAdvanced Synthesis &Catalysis, Volume 367, Issue 5, March 4, 2025.
Abstract While arylazo sulfones have been widely applied as arylating agents, their exploitation for diazenylation reactions has been previously limited to electron‐rich alkenes such as styrenes and silyl enol ethers. Herein we optimized a synthetic one‐pot protocol to access oxazolyl azo compounds via a selective domino ring‐closing/aryldiazenylation ...
Enzo Delalande   +5 more
wiley   +1 more source

Visible Light‐Promoted Esterification of Carboxylic Acids via Photoacid Generation Catalysis

open access: yesAdvanced Synthesis &Catalysis, EarlyView.
A novel, environmentally friendly photochemical method for the esterification of carboxylic acids with alcohols using arylazo sulfones as photoacid generators was developed. This approach avoids traditional acidic catalysts, purification did not require chromatography and the method proved effective under continuous flow conditions for enhanced ...
Valentina Benazzi   +7 more
wiley   +1 more source

Synthesis of Spirolactones from Carbonyls via Carboborylation of N‐Sulfonylhydrazones with Alkoxycarbonylalkylboronic Acids

open access: yesAdvanced Synthesis &Catalysis, EarlyView.
Spirolactones are readily prepared from carbonyls via their N‐tosylhydrazones. The reaction involves carboborylation with ethoxycarbonyl‐substituted boronic acids, followed by oxidation and lactonization. Thermal or photochemical protocols enable versatility.
Lucía López   +3 more
wiley   +1 more source

eAmidation: An Electrochemical Amidation of Aldehydes via the Oxidation of N‐Aryl Hydrazones

open access: yesAdvanced Synthesis &Catalysis, EarlyView.
The indirect electrochemical oxidation of N‐aryl hydrazones offers an efficient approach to access amides from aldehydes and amines. The AZADO‐mediated reaction enables the selective synthesis of a broad range of valuable amides using readily available aldehydes.
Luke Chen   +2 more
wiley   +1 more source

A case report of acute interstitial nephritis caused by cotton phenol. [PDF]

open access: yesBMC Urol
Zhao M   +7 more
europepmc   +1 more source

C–H Homocoupling of Arenes via Pd/S,O‐Ligand Catalysis

open access: yesAdvanced Synthesis &Catalysis, EarlyView.
An efficient C‐H homocoupling of arenes via Pd/S,O‐ligand catalytic system is reported. This method can be applied to a series of arenes using O2 as oxidant under room temperature and is also applicable for late‐stage homocoupling of pharmaceutical derivatives.
Ke‐Zuan Deng   +3 more
wiley   +1 more source

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