Results 111 to 120 of about 25,595 (290)

Bayesian Optimization of Solvent‐Free Thermal Amidation via Reactive Extrusion

Chemistry – A European Journal, EarlyView.
Thermal amidation between a carboxylic acid and an amine was successfully conducted in an extruder in the absence of solvent, coupling agent, or catalyst, relying on an adapted Bayesian Optimization protocol. Active pharmaceutical ingredient moclobemide was synthesized on a larger scale, achieving excellent yield and low Process Mass Intensity (PMI ...
Matthieu Lavayssiere, Xavier Bantreil, Frédéric Lamaty   +2 more
wiley   +1 more source

Mechanochemically Synthesized CIGS Nanocrystalline Powder for Solar Cell Application [PDF]

, 2013
Copper Indium Gallium Diselenide (CIGS) is a compound semiconductor material from the group of I-III-VI. The material is a solid solution of copper, indium and selenium (CIS) and copper, gallium and selenium with an empirical formula of CuIn(1 – x)GaxSe2,
Desai, R.R., Master, Hamza, Panchal, C.J., Patel, P.B., Ray, J.R., Rehani, Bharati   +5 more
core  

A Fast and Highly Stable Aqueous Calcium‐Ion Battery for Sustainable Energy Storage

ChemSusChem, Volume 18, Issue 6, March 15, 2025.
Aqueous batteries provide a low‐cost, safer alternative to lithium‐ion batteries, but their viability is often limited by rapid electrode degradation. This study shows that replacing K+ with divalent Ca2+ ions in the electrolyte significantly boosts the stability of both copper hexacyanoferrate cathodes and polyimide anodes, enabling fast‐charging ...
Raphael L. Streng, Samuel Reiser, Sabrina Wager, Nykola Pommer, Aliaksandr S. Bandarenka   +4 more
wiley   +1 more source

X-ray diffraction and Mössbauer spectroscopy studies of a mechanosynthesized Fe75B25 alloy

Nukleonika, 2015
In this work, the process of formation of metastable phases was investigated for the Fe75B25 composition. Mechanical synthesis was performed in a MAPF-2M high-energy planetary ball mill under an argon atmosphere.
Jartych Elżbieta, Kubalova Ludmila M., Fadeeva Victoria I.   +2 more
doaj   +1 more source

Synthesis and structural evolution of vanadium carbide in nano scale during mechanical alloying

Journal of King Saud University: Engineering Sciences, 2016
In this study, nano crystalline vanadium carbide was synthesized by mechanical alloying method. V2O5, C and Mg powders were placed in a planetary ball mill and sampled after different milling times.
Mohsen Hossein-Zadeh, Mansour Razavi, Mohsen Safa, Amin Abdollahi, Omid Mirzaee   +4 more
doaj   +1 more source

Lithium Sulphur Batteries [PDF]

, 2015
S+C cathode material was prepared by simple solid-state reaction in ball mill. Content of sulphur was approximately 80 wt. % in final sample. Cyclic voltammetry and galvanostatic charge/discharge techniques were used for characterization of the samples ...
Juračka, M.
core  

Comparative Analysis of Metal Preloading Technologies in Batteries and Capacitors

EcoEnergy, EarlyView.
Metal preloading strategies play an important role in efficient batteries and hybrid capacitors to compensate for the consumed metals at the first discharge. This article reviews recent progress in preloading technologies in lithium‐ion and other metal‐ion systems.
Xuexue Pan, Yu Zhang, Zhazira Supiyeva, Qamar Abbas   +3 more
wiley   +1 more source

A Review of Grain Boundaries: Formation Mechanism, Synthesis Strategy, and Application in Electrocatalysis

EcoEnergy, EarlyView.
An overview of grain boundary engineering in the field of electrocatalysis. ABSTRACT Key electrocatalytic reactions such as HER, OER, ORR, CO2RR, and NRR offer promising routes for storing renewable energy as chemical fuels. However, their widespread application is constrained due to the lack of highly active and stable catalysts. Grain boundaries (GBs)
Jingyu Gao, Fengming Zhou, Xinying Li, Ying Deng, Zexing Wu, Siyuan Feng, Yujing Zhu, Dan Zhang, Zhenyu Xiao   +8 more
wiley   +1 more source

Mechanochemical Synthesis of Lead-Free Halide Layered Double Perovskites: A Green and Scalable Approach. [PDF]

ChemSusChem
Herein we report a facile, green, and scalable synthetic alternative for the obtention of layered double perovskites (LDPs) via mechanosynthesis. This approach allows for the synthesis of phase‐pure LDPs in batches of up to 5 g within minutes. To our knowledge, this represents the largest scale and fastest synthesis of these materials reported to date.
Escobedo-Perez TI, Osorio-Sotelo R, Solis-Ibarra D.   +2 more
europepmc   +2 more sources

A Review of Black Phosphorus‐Based Materials: From Preparation Strategies to Characterization Techniques

ENERGY &ENVIRONMENTAL MATERIALS, EarlyView.
The structure, properties, preparation methods, and characterization techniques of BP. As a typical 2D layered material, black phosphorus (BP) demonstrates exceptional promise in various fields, particularly in energy storage for alkali metal‐ion batteries. However, its distinctive structure and properties, together with the compositional complexity of
Yunqing Wang, Jinzhi Lyu, Yongxiang Li, Yubing Wang, Xiangming Cui, Jianan Wang, Banglong Wan, Wei Yan   +7 more
wiley   +1 more source