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WPPM: Microstructural Analysis beyond the Rietveld Method
Materials Science Forum, 2010The basics of the Whole Powder Pattern Modeling and its implementation in the PM2K software are briefly reviewed. The main features and functionalities, and most common line broadening models are introduced with the aid of working examples related to the instrumental profile and to a plastically deformed metal.
Scardi, Paolo +2 more
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An alternative to the Rietveld profile refinement method
Zeitschrift für Kristallographie - Crystalline Materials, 1981Abstract A new method (SCRAP) has been used for the analysis of neutron powder diffraction data as an alternative to the Rietveld profile refinement method, which has been shown to give incorrect values for the standard deviations of the parameters.
M. J. Cooper, K. D. Rouse, M. Sakata
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An analysis of the Rietveld refinement method
Journal of Applied Crystallography, 1979An analysis of the Rietveld profile refinement method used in the interpretation of neutron or X-ray powder diffraction patterns has been carried out. It is shown that the values obtained for the structural parameters are not exactly the same as those obtained from an integrated intensity refinement of the same data and that the standard deviations of ...
M. Sakata, M. J. Cooper
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The validity of the Rietveld method
Zeitschrift für Kristallographie - Crystalline Materials, 1983Abstract The values of the estimated standard deviations given by the Rietveld profile refinement method are formally invalid, since the method does not take into account systematic errors which are introduced into the residuals by the constraints of the model from which the calculated intensities are derived.
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Structure of Carbonated Hydroxyapatite Based on Rietveld Method
Key Engineering Materials, 2008The crystalline structures of B-type carbonated hydroxyapatite (CHA) powders sintered at 700, 900 and 1100°C, respectively, were studied by Rietveld analysis of powder X-ray diffraction (XRD) data. A series of structure parameters, including lattice parameters (a and c), bond length and the distortion index of PO4 tetrahedron (Dind) were calculated by ...
Xu Ran +4 more
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1993
Abstract The Rietveld method is a powerful and relatively new method for extracting detailed crystal structural information from X-ray and neutron powder diffraction data. Since such structural details dictate much of the physical and chemical attributes of materials, knowledge of them is crucial to our understanding of those ...
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Abstract The Rietveld method is a powerful and relatively new method for extracting detailed crystal structural information from X-ray and neutron powder diffraction data. Since such structural details dictate much of the physical and chemical attributes of materials, knowledge of them is crucial to our understanding of those ...
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Amorphous/nanocrystalline composites analysed by the Rietveld method
Journal of Alloys and Compounds, 2010The Rietveld refinement approach has been applied to semi-crystalline materials in the case of bulk metallic glasses. Specifically, the crystallisation behaviour of a Fe48Cr15Mo14Y2C15B6 bulk metallic glass has been investigated by in situ X-ray diffraction obtained using a high intensity monochromatic synchrotron beam at the ID11 line of ESRF in ...
BARICCO, Marcello +5 more
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Crystal structure of LaVO3 by Rietveld refinement method
Materials Letters, 2004Abstract Structure refinement of LaVO 3 was carried out using the whole pattern fitting or Rietveld method, which is a powerful technique for extracting structural information from powder diffraction data. The crystal structure refinement was done using powder X-ray diffraction data measured on a conventional diffractometer.
R.T.A. Khan +3 more
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Simultaneous structure and size–strain refinement by the Rietveld method
Journal of Applied Crystallography, 1990A new procedure for simultaneous refinement of structural and microstructural disorder parameters for polycrystalline materials is proposed. It is based on the Rietveld method combined with Fourier analysis for broadened peaks. Crystallite size and shape and r.m.s.
Lutterotti, Luca, Scardi, Paolo
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Size-Strain and Quantitative Phase Analysis by the Rietveld Method
Advances in X-ray Analysis, 1991AbstractA modified version of the Rietveld method has been developed for quantitative phase analysis in conjunction with crystallite size and microstrain determination.Besides the information on the microstructural disorder in the different phases present in the sample, accurate phase analysis can be performed, even in presence of anisotropic ...
Scardi, Paolo +2 more
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