Results 71 to 80 of about 18,381 (288)

Single Crystals of Perylene Diimide‐Based Two‐Dimensional Covalent Organic Frameworks

open access: yesAdvanced Materials, EarlyView.
Synthesizing extended crystals of two‐dimensional covalent organic frameworks (2D COFs) has remained a major challenge. Here, we report a high‐temperature double‐modulator strategy that provides access to new perylene diimide (PDI)‐based COFs with crystal sizes of up to 50 µm.
Ling Zhang   +12 more
wiley   +1 more source

The Rietveld method applied to the quantitative mineralogical analysis of some soil samples from Argentina Aplicación del método de Rietveld al análisis mineral��gico cuantitativo de algunas muestras de suelos de la Argentina

open access: yesCiencia del Suelo, 2007
The mineralogical quantification of soils species is mainly obtained by analysis of X-ray diffraction (XRD) patterns. The classic method, for these analyses, is limited to semi quantitative determinations due to the overlapping of different specie's ...
Stella M Zabala   +3 more
doaj  

Quantitative phase analysis of anhydrous clinker Portland using Rietveld method

open access: yes
Modern cements are complex materials with well-defined compositions that reach to high and consistent results. Automated techniques such as Rietveld analysis lead to provide an understanding of the composition and polymorphism of cement phases that could
Slassi, Siham   +5 more
core   +1 more source

Mechanical Stress Evolution in Polycrystalline Ge Thin Films Under MeV Ion Irradiation

open access: yesAdvanced Materials Interfaces, EarlyView.
Irradiation of polycrystalline Ge thin films with 1.8 MeV Au ions alters residual stress through defect generation and lattice expansion. Increasing fluence drives progressive lattice disorder and eventual amorphization. Polycrystalline Ge resists amorphization longer than crystalline Ge, as grain boundaries facilitate defect diffusion, significantly ...
Karla J. Paz Corrales   +10 more
wiley   +1 more source

Caracterização estrutural da cerâmica Ti x(Sm0,2Ce0,8)1-xO 2-delta pelo método de Rietveld Structural study of Ti x(Sm0.2Ce0.8 )1-xO2-delta ceramic by the Rietveld method

open access: yesCerâmica, 2007
O método precursor polimérico foi aplicado para a síntese de pós de Ti x(Sm0,2Ce0,8)1 xO2-delta, com 0 < x < 0,5, com tratamento nas temperaturas de 400 ºC, 700 ºC e 1000 ºC.
S. Domingues   +4 more
doaj   +1 more source

How Crystalline is My Cellulose Specimen? Probing the Limits of X-ray Diffraction

open access: yesBioResources, 2022
Cellulose serves as a skeleton for many of the useful products upon which we rely on each day. When we want to learn about a skeleton, it makes sense to think about X-ray methods.
Alfred D. French
doaj   +2 more sources

Pyrolysis Induced Interphase and Structural Stabilization of Silicon‐Tin Disulfide/PAN Composite Electrode Materials for Li‐Ion Batteries

open access: yesAdvanced Materials Interfaces, EarlyView.
A Si and SnS2 based dual‐alloy anode material for metal‐ion battery applications with improved structural, interfacial and electrochemical properties is synthesized via a single‐step solid‐state pyrolysis process. During the pyrolysis step, SnS2 and Si are embedded in a porous, carbonized PAN‐based matrix, which is electronically and ionically ...
Akzhan Bekzhanov   +2 more
wiley   +1 more source

3D Printing of Highly Dense and Translucent Zirconia Parts for Dental Applications: Effect of Filament Overlapping

open access: yesAdvanced Materials Technologies, EarlyView.
This study formulated a 5Y‐PSZ zirconia paste for extrusion‐based additive manufacturing via direct ink writing, producing dense ceramic structures for dental applications. A colloidal approach with 47 vol% nanometric powder and tailored additives optimized rheology and printability.
Juliana de Freitas Gouveia Silva   +5 more
wiley   +1 more source

Crystal structure refinements - Rietveld Method

open access: yes, 2017
The talk is an introduction into the Rietveld method and basic aspects concerning powder diffraction analysis. The FOX- and Jana software are explained stepwise which should enable the audiences of the talk to start structure refinements by their ...
Schlegel, Moritz-Caspar, Svetogorov, R.
core  

The Influence of Mesoscale Particle Structure on the Electrode Degradation and Resultant Electrochemistry of Lithium Ion Cells With Nickel Rich Lithium Nickel Manganese Cobalt Oxide Positive Electrodes

open access: yesAdvanced Materials Technologies, EarlyView.
Milled polycrystalline NMC811 cathode (MPC NMC) with smaller secondary particle and higher surface area had 1) greater cathode tortuosity, 2) reduced surface Ni on the cycled MPC cathodes consistent with surface reconstruction, and 3) increased Ni deposition from cathode‐anode crosstalk, manifesting in lower functional capacity and higher impedance ...
Edelmy J. Marin Bernardez   +22 more
wiley   +1 more source

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