Neutron and X-ray powder diffraction data to determine the structural properties of novel layered perovskite PrSrMn2O5+δ [PDF]
The data presented in this article are related to the formation of a novel layered perovskite oxide material, PrSrMn2O5+δ, through a solid-state synthesis route.
Shammya Afroze +5 more
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“Everything's a sample”: Characterizing everyday materials using x-ray powder diffraction [PDF]
We can learn something scientifically interesting about literally everything around us by examining it in a powder diffractometer. Comparing a macroscopic understanding of a material with the atomic-scale description proves to be a good way of generating
James A. Kaduk
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Omadacycline dihydrate, C29H40N4O7·2H2O, from X-ray powder diffraction data [PDF]
The crystal structure of the title compound {systematic name: (4S,4aS,5aR,12aR)-4,7-bis(dimethylamino)-9-[(2,2-dimethylpropylamino)methyl]-1,10,11,12a-tetrahydroxy-3,12-dioxo-4a,5,5a,6-tetrahydro-4H-tetracene-2-carboxamide dihydrate, C29H40N4O7·2H2O} has
James A. Kaduk +4 more
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Synthesis of Vanadium-Vanadium Carbide in-situ nanocomposites by high energy ball milling and spark plasma sintering [PDF]
In the present work, Vanadium-Vanadium Carbide (V-V2C) in-situ nanocomposites were synthesized by mechanically milling vanadium powders with 0.5 wt.% stearic acid.
Krishnan Vinoadh Kumar +1 more
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X-ray powder diffraction is a vital analytical tool that is used in pharmaceutical science. It is increasingly used to establish the crystal structure of a new pharmaceutical substance, in particular, cocrystal or its polymorphic forms.
Vladimir V. Chernyshev
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Application of X-ray Powder Diffraction Method in Identification and Classification of Leptite
BACKGROUND The identification of leptite is usually based on microscopic identification technology, but it is very difficult to distinguish tiny feldspar, quartz, and layered silicate minerals such as chlorite, montmorillonite and mica using a microscope.
WU Yue, CHI Guang-cheng, LIU Xin
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A carbamazepine-indomethacin (1:1) cocrystal produced by milling [PDF]
An X-ray amorphous mixture of carbamazepine and indomethacin transforms upon annealing to produce a novel 1:1 cocrystal, whose structure has been determined from laboratory powder X-ray diffraction (PXRD ...
Buckton, Graham +6 more
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Synchrotron X-ray powder diffraction [PDF]
The application of synchrotron X-ray radiation to powder diffraction is described. A perfect Si double-crystal monochromator at the Cornell High Energy Synchrotron Source (CHESS) was used in conjunction with Si, Ge, LiF and Al2O3 analyzers to investigate resolution and intensity characteristics at selected wavelengths between 1.07 and 1.54 A.
W. Parrish, M. Hart, T. C. Huang
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Acemetacin cocrystal structures by powder X-ray diffraction
Cocrystals of acemetacin drug (ACM) with nicotinamide (NAM), p-aminobenzoic acid (PABA), valerolactam (VLM) and 2-pyridone (2HP) were prepared by melt crystallization and their X-ray crystal structures determined by high-resolution powder X-ray ...
Geetha Bolla +2 more
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Zeolite phi: a physical mixture of chabazite and offretite [PDF]
Zeolite Phi is synthesized by two methods reported previously. Results from X-ray powder diffraction and scanning electron microscopy suggest that the materials are physical mixtures of chabazite and offretite; one sample has a small amount of ...
Annen, Michael J. +2 more
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