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Application of X-ray Powder Diffraction Method in Identification and Classification of Leptite
BACKGROUND The identification of leptite is usually based on microscopic identification technology, but it is very difficult to distinguish tiny feldspar, quartz, and layered silicate minerals such as chlorite, montmorillonite and mica using a microscope.
WU Yue, CHI Guang-cheng, LIU Xin
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By using the most popular method of thermal condensation of dicyandiamide in a semi-closed system, graphitic carbon nitrides (gCNs) were synthesized at 500, 550, and 600 °C.
E. Alwin +4 more
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Acemetacin cocrystal structures by powder X-ray diffraction
Cocrystals of acemetacin drug (ACM) with nicotinamide (NAM), p-aminobenzoic acid (PABA), valerolactam (VLM) and 2-pyridone (2HP) were prepared by melt crystallization and their X-ray crystal structures determined by high-resolution powder X-ray ...
Geetha Bolla +2 more
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Nanocrystalline materials studied by powder diffraction line profile analysis [PDF]
X-ray powder diffraction is a powerful tool for characterising the microstructure of crystalline materials in terms of size and strain. It is widely applied for nanocrystalline materials, especially since other methods, in particular electron microscopy ...
Gubicza, Jenő, Ungár, Tamás
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Sub-nanosecond X-ray powder diffraction
The X-rays emitted from a laser-produced plasma have been used to obtain powder diffraction patterns with exposures of less than a nanosecond. The X-rays were produced by focusing approximately 50 J of 0.53 μm laser light in a 600 ps (FWHM) pulse to a tight (~100 μm diameter) spot on a solid titanium target.
Woolsey, N.C., Wark, J.S., Riley, David
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Characterization of defect structures in nanocrystalline materials by X-ray line profile analysis [PDF]
X-ray line profile analysis is a powerful alternative tool for determining dislocation densities, dislocation type, crystallite and subgrain size and size-distributions, and planar defects, especially the frequency of twin boundaries and stacking faults.
Tamás Ungár +3 more
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X-ray characterization by energy-resolved powder diffraction
A method for single-shot, nondestructive characterization of broadband x-ray beams, based on energy-resolved powder diffraction, is described. Monte-Carlo simulations are used to simulate data for x-ray beams in the keV range with parameters similar to ...
G. Cheung, S. M. Hooker
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Herein a novel inorganic-organic hybrid Keggin-type heteropolymolybdate [Ni2Na(C12H8N2)4(BMo12O40)(H2O)2] (1) has been synthesized under hydrothermal conditions in aqueous solution.
Mükerrem Fındık +4 more
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X-RAY POWDER DIFFRACTION IN QUALITY CONTROL OF MEDICINES
X-ray powder diffraction is one of the methods used for detection and analysis of polymorphic forms of pharmaceutical substances. The article elucidates the concept of polymorphism, briefly explains physical characteristics of this phenomenon, conditions
V. S. Kuzmin +2 more
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Using hydrophilic ionic liquid, [bmim]BF4-ethylene glycol system as a novel media for the rapid synthesis of copper nanoparticles. [PDF]
In this work, we present a novel method for the synthesis of copper nanoparticles. We utilize the charge compensatory effect of ionic liquid [bmim]BF(4) in conjunction with ethylene glycol for providing electro-steric stabilization to copper ...
Manika Dewan +4 more
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