Absence of structural correlations of magnetic defects in heavy fermion LiV2O4
Magnetic defects have pronounced effects on the magnetic properties of the face-centered cubic compound LiV2O4. The magnetic defects arise from crystal defects present within the normal spinel structure.
Das, S. +4 more
core +1 more source
Aerosol-assisted metallo-organic chemical vapour deposition of Bi2Se3 films using single-molecule precursors: the crystal structure of bismuth(m) dibutyldiselenocarbamate [PDF]
The complexes [Bi{Se2CN(C2H5)2}3], [Bi{Se2CN(C4H9)2}3], [Bi{Se2CN(CH3)(C4H9)}3] and [Bi{Se2CN(CH3)(C6H13)}3] have been synthesized and characterized structurally using IR, 1H and 13C NMR.
Klinowski, J +5 more
core +2 more sources
Three B2-type intermetallic AlFe1 – δ phases (0.18 < δ < 0.05) in the Al–Fe binary system were synthesized by smelting and high temperature sintering methods. The exact crystal structure for δ = 0.05 was refined by single-crystal X-ray diffraction.
Yibo Liu +4 more
doaj +1 more source
Transformation of Ammonium Dicyanamide into Dicyandiamide in the Solid [PDF]
Ammonium dicyanamide NH4[N(CN)2] was synthesized through aqueous ion exchange. The crystal structure was investigated by single-crystal X-ray diffraction (P21/c, a = 378.67(6) pm, b = 1240.9(3) pm, c = 911.84(14) pm, β = 91.488(18)°, Z = 4).
Höppe, Henning A. +3 more
core +1 more source
Characterization of Photonic Colloidal Single Crystals by Microradian X‐ray Diffraction [PDF]
Photonic crystals (PCs) can provide unprecedented control over both the emission and the propagation of light, allowing important applications in, for example, infrared telecommunications. [1–3] However, fabrication and characterization of PCs is challenging owing to the large refractive-index contrast that is needed to open up a photonic bandgap.
Thijssen, J.H.J. +6 more
openaire +5 more sources
Laser, vacuum and gas reaction chamber for operando measurements at NSLS-II's 28-ID-2
We present a laser reaction chamber that we have developed for in situ/operando X-ray diffraction measurements at the NSLS-II 28-ID-2 X-ray powder diffraction beamline.
Lauren Y. Moghimi +14 more
doaj +1 more source
Crystal structure and phonon softening in Ca3Ir4Sn13
We investigated the crystal structure and lattice excitations of the ternary intermetallic stannide Ca3Ir4Sn13 using neutron and x-ray scattering techniques. For T > T* ~ 38 K the x-ray diffraction data can be satisfactorily refined using the space group
Cervellino, A. +16 more
core +3 more sources
High-temperature synthesis, single-crystal X-ray and neutron powder diffraction, and materials properties of Sr3Ln10Si18Al12O18N36 (Ln = Ce, Pr, Nd) [PDF]
The novel oxonitridoaluminosilicates (sialons) Sr3Ln10Si18Al12O18N36 (Ln = Ce, Pr, Nd) were obtained by the reaction of the respective lanthanide metals with Si(NH)2, SrCO3, and AlN using a radiofrequency furnace at temperatures between 1550–1650°C.
Henry, Paul F. +4 more
core +1 more source
Crystal structure of apatite type Ca2.49Nd7.51(SiO4)6O1.75
The title compound, Ca2+xNd8–x(SiO4)6O2–0.5x (x = 0.49), was synthesized at 1873 K and rapidly quenched to room temperature. Its structure has been determined using single-crystal X-ray diffraction and compared with results reported using neutron and X ...
Thu Hoai Le +5 more
doaj +1 more source
Nonlinear optical behaviour of bis (cytosinium) tartarate monohydrate single crystal
A nonlinear optical single crystal of bis (cytosinium) tartarate monohydrate (BCTM) was grown by slow evaporation method at room temperature. Single crystal X-ray diffraction study revealed their cell parameters and corresponding space group.
P. Jaikumar +4 more
doaj +1 more source

