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Solid Phase Extraction Troubleshooting
2004Extraction problems that can arise with solid phase extraction are not unlike those that occur with any type of chemical extraction process, including recovery and contamination problems. Since SPE usually requires columnar flow processes, liquid flow problems are possible and more unique to this methodology.
Michael J. Telepchak +2 more
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Solid-phase extraction in clinical biochemistry
Annals of Clinical Biochemistry: International Journal of Laboratory Medicine, 2002In order to measure low concentrations of analytes in plasma and urine, it is often necessary to extract and concentrate them. With solid-phase extraction (SPE), this is achieved by partitioning the analytes between a solid and a liquid or headspace vapour.
Walker, Valerie, Mills, Graham A.
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Solvent-assisted dispersive solid phase extraction
Talanta, 2013In this research, a novel extraction technique termed solvent-assisted dispersive solid phase extraction (SADSPE) was developed for the first time. The new method was based on the dispersion of the sorbent into the sample to maximize the contact surface.
Mohammad Reza, Jamali +2 more
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Solid-Phase Extraction in Malondialdehyde Analysis
Analytical Biochemistry, 1997Malondialdehyde (MDA) has been widely used as an index of lipoperoxidation in biological and medical sciences as well as in the food industry. A solid-phase extraction (SPE) of the condensation product of the MDA with 2-thiobarbituric acid (TBA) was developed using LiChrolut C18ec, 200 mg (Merck, Darmstadt, Germany), as a SPE cartridge and methanol as ...
J, Suttnar, J, Cermák, J E, Dyr
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Solid-phase extraction of acidic herbicides
Journal of Chromatography A, 2000A discussion of solid-phase extraction method development for acidic herbicides is presented that reviews sample matrix modification, extraction sorbent selection, derivatization procedures for gas chromatographic analysis, and clean-up procedures for high-performance liquid chromatographic analysis.
M J, Wells, L Z, Yu
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Solid phase extraction fundamentals
Nature, 1988Sample preparation columns based on the principles of solid phase extraction are fast becoming indispensable tools in many types of research.
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Dispersive-Micro-Solid Phase Extraction
Dispersive extraction techniques are valuable for their ability to maximize the interaction between the sample and the extractant, leading to increased extraction efficiency. Dispersive solid phase extraction (dSPE) was initially developed to enhance the selectivity of the analytical process by using a solid phase to retain potential interferents from ...openaire +2 more sources
DNA Extraction: Organic and Solid-Phase
2016DNA extraction remains a critical step in DNA profiling of biological material recovered from scenes of crime. In the forensic community several methods have gained popularity, including Chelex(®), organic extraction, and solid-phase extraction. While some laboratories streamlined their processes and only use one method we have retained several methods
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