Synthesis of 2-Acylphenol and Flavene Derivatives from the Ruthenium-Catalyzed Oxidative C-H Acylation of Phenols with Aldehydes [PDF]
, 2015 The cationic ruthenium hydride complex [(C6H6)(PCy3)(CO)RuH]+BF4− has been found to be an effective catalyst for the oxidative C–H coupling reaction of phenols with aldehydes to give 2-acylphenol compounds.
Aponick +47 more
core +2 more sources
Spectral Analysis and Structural Elucidation of Luliconazole
Chinese Journal of Magnetic Resonance, 2018 Infrared spectra, ultraviolet spectra, nuclear magnetic resonance (NMR) spectra (i.e., 1H NMR, 13C NMR, DEPT135, 1H-1H COSY, 1H-13C HMQC and 1H-13C HMBC) and mass spectra of luliconazole were collected and used to characterize the compound.
LIN Yun-liang +3 more
doaj +1 more source
Spectroscopic Studies of Delafloxacin Meglumine
Chinese Journal of Magnetic Resonance, 2021 The structure of delafloxacin meglumine was analyzed by infrared absorption (IR), ultraviolet absorption (UV), nuclear magnetic resonance (1H NMR, 13C NMR, DEPT, 1H-1H COSY, 1H-13C HSQC and 1H-13C HMBC) spectroscopy, mass spectrometry and elemental ...
Xin-yi ZHAO +4 more
doaj +1 more source
A Versatile Ligand Platform that Supports Lewis Acid Promoted Migratory Insertion [PDF]
, 2012 A helping hand: Incorporation of Group 2 Lewis acids into a macrocycle appended to a phosphine ligand attached to a rhenium carbonyl complex promotes otherwise unfavorable transformations of coordinated CO (see scheme; M=Ca, Sr).
Bercaw, John E. +2 more
core +1 more source
Rational Design, Synthesis and Biological Evaluation of Pyrimidine-4,6-diamine derivatives as Type-II inhibitors of FLT3 Selective Against c-KIT. [PDF]
, 2018 FMS-like Tyrosine Kinase 3 (FLT3) is a clinically validated target for acute myeloid leukemia (AML). Inhibitors targeting FLT3 have been evaluated in clinical studies and have exhibited potential to treat FLT3-driven AML.
Bharate, Jaideep B +8 more
core +2 more sources
Analyzing Pentaerythritol Stearate Homologs with NMR Spectroscopy
Chinese Journal of Magnetic Resonance, 2018 A pentaerythritol stearate sample with unknown composition was analyzed by nuclear magnetic resonance (NMR) spectroscopy (i.e., 1H NMR, quantitative 13C NMR, DEPT135, 1H-1H COSY, 1H-1H NOESY, 1H-13C HSQC and 1H-13C HMBC).
LI Chun-fa +3 more
doaj +1 more source
Spectral Analyses and Structural Elucidation of Cyflumetofen
Chinese Journal of Magnetic Resonance, 2020 Cyflumetofen is a new type of acaricide with high efficiency and low residue. In this work, the compound was characterized by infrared absorption (IR), ultraviolet absorption (UV) and mass spectrometry, as well as nuclear magnetic resonance spectroscopy (
ZHANG Yi-ming +2 more
doaj +1 more source
Intra- and Intermolecular C−H Activation by Bis(phenolate)pyridineiridium(III) Complexes [PDF]
, 2011 A bis(phenolate)pyridine pincer ligand (henceforth abbreviated as ONO) has been employed to support a variety of iridium complexes in oxidation states I, III, and IV.
Bercaw, John E. +2 more
core +2 more sources
900MHz 1H-/13C-NMR analysis of 2-hydroxyglutarate and other brain metabolites in human brain tumor tissue extracts. [PDF]
PLoS ONE, 2018 PURPOSE:To perform in vitro high-resolution 900 MHz magnetic resonance spectroscopy (NMR) analysis of human brain tumor tissue extracts and analyze for the oncometabolite 2-hydroxyglutarate (2HG) and other brain metabolites, not only for 1H but also for ...
Gregory Hyung Jin Park +2 more
doaj +1 more source
Photochemical Electrocyclic Ring Closure and Leaving Group Expulsion from N-(9-oxothioxanthenyl)Benzothiophene Carboxamides [PDF]
, 2013 N-(9-Oxothioxanthenyl)benzothiophene carboxamides bearing leaving groups (LG− = Cl−, PhS−, HS−, PhCH2S−) at the C-3 position of the benzothiophene ring system photochemically cyclize with nearly quantitative release of the leaving group, LG−.
Sarker, Majher I. +3 more
core +3 more sources