High-resolution solid state NMR experiments for the characterization of calcium phosphate biomaterials and biominerals [PDF]
Calcium phosphates form a vast family of biominerals, which have attracted much attention in fields like biology, medicine, and materials science, to name a few.
Hanna, John +55 more
core +5 more sources
NMR-Based metabolomic studies of breast cancer [PDF]
Breast cancer is the most frequently diagnosed form of cancer and leading cause of cancer death in females. Current screening techniques, such as mammography, are inadequate. Screening reduces the number of deaths caused by breast cancer but also results
Yabsley, Warren
core +6 more sources
An inter-laboratory comparison demonstrates that [H-1]-NMR metabolite fingerprinting is a robust technique for collaborative plant metabolomic data collection. [PDF]
In any metabolomics experiment, robustness and reproducibility of data collection is of vital importance. These become more important in collaborative studies where data is to be collected on multiple instruments.
Biais, Benoit +50 more
core +1 more source
Ex-vivo HRMAS of adult brain tumours: metabolite quantification and assignment of tumour biomarkers [PDF]
Background: High-resolution magic angle spinning (HRMAS) NMR spectroscopy allows detailed metabolic analysis of whole biopsy samples for investigating tumour biology and tumour classification.
B Bell +29 more
core +2 more sources
1H-Detected Solid-State NMR Studies of Water-Inaccessible Proteins In Vitro and In Situ [PDF]
1H detection can significantly improve solid-state NMR spectral sensitivity and thereby allows studying more complex proteins. However, the common prerequisite for 1H detection is the introduction of exchangeable protons in otherwise deuterated proteins,
Daniëls, Mark +15 more
core +1 more source
Solid-state NMR spectroscopy on complex biomolecules [PDF]
Biomolecular applications of NMR spectroscopy are often merely associated with soluble molecules or magnetic resonance imaging. However, since the late 1970s, solid-state NMR (ssNMR) spectroscopy has demonstrated its ability to provide atomic-level ...
NMR Spectroscopy +7 more
core +1 more source
Spectral Analysis and Structural Elucidation of Luliconazole
Infrared spectra, ultraviolet spectra, nuclear magnetic resonance (NMR) spectra (i.e., 1H NMR, 13C NMR, DEPT135, 1H-1H COSY, 1H-13C HMQC and 1H-13C HMBC) and mass spectra of luliconazole were collected and used to characterize the compound.
LIN Yun-liang +3 more
doaj +1 more source
Improvements in Resolution of 1H NMR of solids
Magic angle spinning (MAS) in 1H NMR has allowed progress from featureless spectra in static samples to linewidths of a few hundreds of Hertz for powdered solids at the fastest spinning rates available today (100-150 kHz). While this is a remarkable improvement, this level of resolution is still limiting to the widespread use of 1H NMR for complex ...
de Almeida, Bruno Simoes, Emsley, Lyndon
openaire +2 more sources
Combining NMR spectroscopy and organic synthesis : from small building blocks to large biomolecules [PDF]
Detailed knowledge of the structure of bio molecules with atomic resolution is essential for the understanding of their function. Moreover the identification and quantification of their dynamic processes are important, as they are the origin of molecular
Gsellinger, Heiko
core +1 more source
Spectral Analyses and Structural Elucidation of Cyflumetofen
Cyflumetofen is a new type of acaricide with high efficiency and low residue. In this work, the compound was characterized by infrared absorption (IR), ultraviolet absorption (UV) and mass spectrometry, as well as nuclear magnetic resonance spectroscopy (
ZHANG Yi-ming +2 more
doaj +1 more source

