Synthesis, Crystal Structure, and Solid-State NMR Investigations of Heteronuclear Zn/Co Coordination Networks - A Comparative Study [PDF]
Synthesis and solid-state NMR characterization of two isomorphous series of zinc and cobalt coordination networks with 1,2,4-triazolyl benzoate ligands are reported. Both series consist of 3D diamondoid networks with four-fold interpenetration.
Baias, M +10 more
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Structural Elucidation and NMR Spectral Assignments of Two C19-Diterpenoid Alkaloids
Two C19-diterpenoid alkaloids, homochasmanine (compound 1) and 14-debenzoylfranchetine (compound 2), were isolated from the roots of Aconitum handelianum. Their structures were elucidated by one-dimensional and two-dimensional nuclear magnetic resonance (
YIN Tian-peng +4 more
doaj +1 more source
900MHz 1H-/13C-NMR analysis of 2-hydroxyglutarate and other brain metabolites in human brain tumor tissue extracts. [PDF]
PURPOSE:To perform in vitro high-resolution 900 MHz magnetic resonance spectroscopy (NMR) analysis of human brain tumor tissue extracts and analyze for the oncometabolite 2-hydroxyglutarate (2HG) and other brain metabolites, not only for 1H but also for ...
Gregory Hyung Jin Park +2 more
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Controlling the Morphology of Aggregates of an Amphiphilic Synthetic Receptor through Host-Guest Interactions [PDF]
A new amphiphilic receptor containing a macrocyclic anionic headgroup and a single alkyl chain was prepared through an efficient templated synthesis. The interdependence of the aggregation behavior and the host-guest chemistry was studied. In the absence
Chhabra, Anjali, +6 more
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The nucleoside derivative N-isobutyryl-3'-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-2'-benzyloxy carbonyl-guanosine (compound 1) was obtained by selectively cleaving the 1,1,3,3-tetraisopropyldisiloxanyl protecting group at 5'-position with
WEI Hui-qiang +5 more
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A Versatile Ligand Platform that Supports Lewis Acid Promoted Migratory Insertion [PDF]
A helping hand: Incorporation of Group 2 Lewis acids into a macrocycle appended to a phosphine ligand attached to a rhenium carbonyl complex promotes otherwise unfavorable transformations of coordinated CO (see scheme; M=Ca, Sr).
Bercaw, John E. +2 more
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Synthesis of 2-Acylphenol and Flavene Derivatives from the Ruthenium-Catalyzed Oxidative C-H Acylation of Phenols with Aldehydes [PDF]
The cationic ruthenium hydride complex [(C6H6)(PCy3)(CO)RuH]+BF4− has been found to be an effective catalyst for the oxidative C–H coupling reaction of phenols with aldehydes to give 2-acylphenol compounds.
Aponick +47 more
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Spectral data of nicotabaflavonoidglycoside
The dataset addressed in this article relates to the research article entitled“Nicotabaflavonoidglycoside, the first example of cembranoid and flavonoid heterodimer from Nicotiana tabacum” (Yang et al., 2018) [1]. The dataset presents the MS4(879-571-421-
Cai-Yan Yang +5 more
doaj +1 more source
Novel 1,3-thiazolidin-4-one derivatives as promising anti-Candida agents endowed with anti-oxidant and chelating properties [PDF]
Pursuing our recent outcomes regarding the antifungal activity of N-substituted 1,3-thiazolidin-4-ones, we synthesized thirty-six new derivatives introducing aliphatic, cycloaliphatic and heteroaromatic moieties at N1-hydrazine connected with C2 position
Abdurrahman, Aktumsek +10 more
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In this paper, one-dimensional (1H NMR, 13C NMR, DEPT, and 19F NMR) and two-dimensional NMR (1H-1H COSY, 1H-13C HMBC, and 1H-13C HSQC) techniques were applied to perform structural identification and NMR spectral assignments of the fluorine-containing ...
ZHENG Jiaqi +3 more
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