Results 151 to 160 of about 208,364 (208)
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On-line sample treatment—capillary gas chromatography
Chromatographia, 1998Sample pretreatment is often the bottleneck of a tracelevel analytical procedure. In order to increase performance, increasing attention is therefore being devoted to combining sample pretreatment on-line with the separation technique that has to be used.
Goosens, E.C. +3 more
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Capillary gas chromatography of azaarenes
Journal of Chromatography A, 1982Abstract Reproducible methods for the preparation of non-polar, medium-polar and polar capillary columns with suitable wall surface deactivation for the analysis of nitrogen bases are described. Parameters affecting deactivation, efficiency and thermal stability are discussed.
J.M. Schmitter +2 more
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Capillary gas-solid chromatography
Russian Chemical Reviews, 1996The current state of gas adsorption chromatography on open tubular capillary columns is analysed. The history of the development of this method and its role in gas chromatography are considered. The preparation of open tubular adsorption capillary columns, fundamentals of the theory of retention and of broadening of chromatographic zones, and the use ...
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Capillary gas chromatography of carbolines
Journal of Chromatography A, 1982Abstract A method was developed for the gas chromatographic analysis of carbolines (pyridoindoles) on fused-silica glass capillary columns, coated with SuperoxTM-4. Separation characteristics are presented for all four possible isomers of carboline and several methyl-, methoxy- and dihydro-derivatives fo β-carboline (norharman).
M.E. Snook, O.T. Chortyk
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Capillary gas chromatography of lupin alkaloids
Journal of Chromatography A, 1983The resolution and identification of twelve lupin alkaloids are demonstrated using capillary gas chromatography and gas chromatography-mass spectrometry. The quantitative capabilities of capillary gas chromatography are illustrated by specific reference to the four major alkaloids of lupinus angustifolius, namely lupanine, 13-hydroxylupanine ...
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Journal of Chromatography A, 2008
The constituents in synthetic alkylbenzene samples were analyzed by a comprehensive capillary liquid chromatography (micro-LC) x capillary gas chromatography (CGC). The micro-LC separates the mixture into aliphatic compounds, monosubstituted alkylbenzenes, multisubstituted alkylbenzenes and binuclear aromatic compounds.
Yuan, Xu +3 more
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The constituents in synthetic alkylbenzene samples were analyzed by a comprehensive capillary liquid chromatography (micro-LC) x capillary gas chromatography (CGC). The micro-LC separates the mixture into aliphatic compounds, monosubstituted alkylbenzenes, multisubstituted alkylbenzenes and binuclear aromatic compounds.
Yuan, Xu +3 more
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Introduction to pyrolysis–capillary gas chromatography
Journal of Chromatography A, 1999By breaking large molecules into characteristic smaller fragments, analytical pyrolysis extends the use of gas chromatography to the analysis of polymeric materials, including natural polymers such as cellulose as well as synthetics. An understanding of the chemistry involved permits interpretation of the information present in these molecular ...
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Pulse circulation gas chromatography on capillary columns
Talanta, 1987The method and equipment for pulse circulation high-resolution gas chromatography on glass capillary columns have been developed. The separation of a mixture of C(6)H(6), C(6)H(5)D, C(6)H(3)D(3) and C(6) D(6) on carbonized columns coated with squalane has been taken as an example to show the advantages of the method.
V P, Chizhkov +5 more
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Wetting Phenomena in Gas Chromatography Capillary Columns
Nature, 1962IN some instances poor efficiency with capillary columns has been reported, especially when glass capillaries were used. This may be due to two quite different phenomena : bad liquid-phase distribution on the smooth wall of the capillary caused by non-uniformity of radius, or non-wetting properties of the stationary phase.
F, FARRE-RIUS, J, HENNIKER, G, GUIOCHON
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Arsenic Speciation by Capillary Gas-Liquid Chromatography
Journal of Chromatographic Science, 1987Specific environmentally significant arsenic compounds are determined by capillary gas-liquid chromatography. Inorganic (arsenite, arsenate) and organic (monomethylarsonate, dimethylarsinate) arsenicals are measured as the corresponding methylthioglycolate derivatives, which are simultaneously separated on wide-bore borosilicate glass and fused-silica ...
K, Dix, C J, Cappon, T Y, Toribara
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