Results 31 to 40 of about 24,605 (215)

Microextraction and Eco-Friendly Techniques Applied to Solid Matrices Followed by Chromatographic Analysis

Separations
In this review, a 5-year overview on environmentally friendly approaches for the extraction of the most relevant organic pollutants in soil, sediment, particulate matter, and sewage sludge coupled with chromatographic analysis is reported.
Attilio Naccarato, Rosangela Elliani, Antonio Tagarelli   +2 more
doaj   +1 more source

Microextraction Techniques Coupled to Liquid Chromatography with Mass Spectrometry for the Determination of Organic Micropollutants in Environmental Water Samples

Molecules, 2014
Until recently, sample preparation was carried out using traditional techniques, such as liquid–liquid extraction (LLE), that use large volumes of organic solvents.
Mª Esther Torres Padrón, Cristina Afonso-Olivares, Zoraida Sosa-Ferrera, José Juan Santana-Rodríguez   +3 more
doaj   +1 more source

Comparative Study of Free and Total Fatty Acids of Spreadable Cheeses by Mass Spectrometry Methods

ChemFoodChem, EarlyView.
This study focuses on the determination of FFAs in spreadable cheeses and alternatives using a fast Liquid Chromatography‐High Resolution Mass Spectrometry method. A Gas Chromatography‐Mass Spectrometry method was used to determine the composition (%) of total FAs in the same samples.
Christiana Mantzourani, Georgia Koutsouridou, Eleftheria H. Kaparakou, Dimitra Daferera, Petros A. Tarantilis, Golfo Moatsou, Maroula G. Kokotou   +6 more
wiley   +1 more source

Application of liquid-phase microextraction to the analysis of trihalomethanes in water

Analytica Chimica Acta, 2006
A liquid-phase microextraction method for the determination of trihalomethanes (THMs) including chloroform (CHCl3), bromodichloromethane (CHBrCl2), dibromochloromethane (CHBr2Cl) and bromoform (CHBr3) in water samples was developed, with analysis by gas chromatography-electron capture detection (GC-ECD).
Tor, Ali, Aydın, M. Emin
openaire   +2 more sources

Cortiça: uma nova abordagem como fase extratora para microextração em fase sólida e microextração em barra adsortiva [PDF]

, 2015
Tese (doutorado) - Universidade Federal de Santa Catarina, Centro de Ciências Físicas e Matemáticas, Programa de Pós-Graduação em Química, Florianópolis, 2015.Neste estudo foi proposto pela primeira vez o uso da cortiça como fase extratora para duas ...
Dias, Adriana Neves
core  

Valproic acid extraction methods in human samples for gas chromatography analysis: a review

Drug Analytical Research
Valproic acid (VPA) is widely used as an important drug for the treatment of epilepsy, seizures, bipolar disorders, and migraines. However, its narrow therapeutic range lead to risks of unintentional poisoning and potential suicide.
Juliana Blume de Oliveira, Bruno Pereira dos Santos, Marcelo Arbo   +2 more
doaj   +1 more source

Micro‐QuEChERS Extraction for Broad‐Spectrum LC‐QQQ‐MS Quantification of Nitazene Analogs in Plasma: A Validated Method With Casework Application

Drug Testing and Analysis, EarlyView.
Micro‐QuEChERS sample preparation coupled to LC‐QQQ‐MS enabled sensitive quantification of nitazene analogs in 100 μL of plasma. The validated method provided low detection limits and was successfully applied to an authentic intoxication case involving N‐pyrrolidino protonitazene, supporting clinical and forensic toxicology workflows.
Karla A. O. Souza, Náthaly C. B. F. Santos, Rafael Lanaro, Sara E. Walton, Alex J. Krotulski, Barry K. Logan, Mauricio Yonamine, Jose Luiz Costa   +7 more
wiley   +1 more source

Advances in Solid-Phase Microextraction [PDF]

, 2020
Analysis imposes substantial challenges, especially when dealing with analytes present at trace levels in complex matrices. Although modern instrumentation has simplified analyses and makes them more reliable, its use is only the last step of the whole ...

core   +4 more sources

Sample treatment platform for automated integration of microextraction techniques and liquid chromatography analysis

HardwareX, 2019
Sample preparation performance influences the quality of every chemical analysis. Since it is the most labor-intensive stage in the nearly all-analytical protocols, sample preparation automation would be desirable, to increase the analytical throughput ...
Deyber Arley Vargas Medina, Luís Felipe Rodriguez Cabal, Fernando Mauro Lanças, Álvaro José Santos-Neto   +3 more
doaj   +1 more source

Cyclodextrins as Chiral Selectors in Capillary Electrophoresis—Recent Developments in Understanding Analyte Complexation and Applications in Pharmaceutical Analysis

ELECTROPHORESIS, EarlyView.
Cyclodextrins are the most often applied chiral selectors in CE enantioseparations. In combination with NMR spectroscopy and molecular modeling, studies for an understanding of chiral recognition underlying enantioseparations have been performed.
Gerhard K. E. Scriba
wiley   +1 more source