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Personalization of pharmacotherapy with sirolimus based on volumetric absorptive microsampling (VAMS) in pediatric renal transplant recipients-from LC-MS/MS method validation to clinical application. [PDF]
Pharmacol RepKocur A +7 more
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A high-performance liquid chromatography method validation and a Box-Behnken experimental design for the extraction optimization of quercitrin from Nectandra reticulata. [PDF]
RSC AdvPulido Teuta J +2 more
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Validation of Bioanalytical Methods
Pharmaceutical Research, 1991Validation of bioanalytical methods used to generate data for pharmacokinetic and bioavailability studies is approached by a variety of techniques and is subject to many different methods of interpretation. This Review puts the various techniques into perspective and discusses pitfalls which may occur in interpretation of validation data.
H T, Karnes, G, Shiu, V P, Shah
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Forensic Science International, 2007
Reliable analytical data are a prerequisite for correct interpretation of toxicological findings in the evaluation of scientific studies, as well as in daily routine work. Unreliable analytical data might not only be contested in court, but could also lead to unjustified legal consequences for the defendant or to wrong treatment of the patient ...
Frank T, Peters +2 more
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Reliable analytical data are a prerequisite for correct interpretation of toxicological findings in the evaluation of scientific studies, as well as in daily routine work. Unreliable analytical data might not only be contested in court, but could also lead to unjustified legal consequences for the defendant or to wrong treatment of the patient ...
Frank T, Peters +2 more
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Practical method validation: Validation sufficient for an analysis method
Mikrochimica Acta, 1998Validation of an analysis method depends on the purpose of the method, the chosen technique and the procedure in question. Methods are used for different research, product development, process control and quality control purposes. The human and economical importance of results vary. Each of the techniques used, such as chromatography-(HPLC, HRGC, TLC),
P. Bruce, P. Minkkinen, M. -L. Riekkola
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Journal of Mathematical Psychology, 2000
This paper gives a review of cross-validation methods. The original applications in multiple linear regression are considered first. It is shown how predictive accuracy depends on sample size and the number of predictor variables. Both two-sample and single-sample cross-validation indices are investigated. The application of cross-validation methods to
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This paper gives a review of cross-validation methods. The original applications in multiple linear regression are considered first. It is shown how predictive accuracy depends on sample size and the number of predictor variables. Both two-sample and single-sample cross-validation indices are investigated. The application of cross-validation methods to
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Validation of Computational Methods
2016In this chapter, we provide an overview of how (Quantitative) Structure Activity Relationships, (Q)SARs, are validated and applied for regulatory purposes. We outline how chemical categories are derived to facilitate endpoint specific read-across using tools such as the OECD QSAR Toolbox and discuss some of the current difficulties in addressing the ...
Grace, Patlewicz +2 more
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Validation of the revised STIr method
Speech Communication, 2002Summary: The revised model for the speech transmission index (STI\(_{r}\)), Speech Communication 28 (1999) 109), was validated with an independent set of 68 test conditions. For a subset of 18 conditions, including only additive noise and band-pass limiting, it was verified that the STI\(_{r}\) provides a good prediction of the CVC-word score.
Steeneken, H.J.M., Houtgast, T.
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2023
In Part II we have introduced the field-theoretic method of study of phase transformations and explored many of its properties. We saw how it can help us better understand the transformations at equilibrium and in dynamics. As materials science is moving into a new era of quantitative modeling and design of real materials, it is important to validate ...
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In Part II we have introduced the field-theoretic method of study of phase transformations and explored many of its properties. We saw how it can help us better understand the transformations at equilibrium and in dynamics. As materials science is moving into a new era of quantitative modeling and design of real materials, it is important to validate ...
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Method validation in the bioanalytical laboratory
Journal of Pharmaceutical and Biomedical Analysis, 1990Bioanalytical methods, based on a variety of physico-chemical and biological techniques such as chromatography, immunoassay and mass spectrometry, must be validated prior to and during use to engender confidence in the results generated. The fundamental criteria for assessing the reliability and overall performance of a bioanalytical method are: the ...
A R, Buick +4 more
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