Results 121 to 130 of about 14,605 (233)

Total X‐Ray Illumination for Absolute Quantification of Crystalline Phases and Amorphous Content in PVDF and P(VDF‐TrFE)

open access: yesMacromolecular Materials and Engineering, EarlyView.
A rigorous method, Total Illumination by X‐rays (TIX), is presented to quantify crystalline and amorphous phases in organic materials. Mitigating challenges such as low microabsorption and high amorphous content, an improved, general framework is established, applicable to polymers, MOFs, biological materials, etc.
Shaashwat Saraff   +2 more
wiley   +1 more source

Hydrogen Bonding Network in Interlayer Spaces of a Partially Deuterated Layered α‐Sn (IV) Phosphate: A Solid‐State MAS NMR Study

open access: yesMagnetic Resonance in Chemistry, EarlyView.
The solid‐state 1H and 2H NMR data collected for deuterated α‐Sn (HPO4)2 phosphate suggest the hydrogen bonding network, where the cavity water accepts one hydrogen bond from the P‐OH donor group and forms one hydrogen bond with the neighboring phosphate group, while the other water hydrogen is not involved in hydrogen bonding.
Vladimir I. Bakhmutov, Hong‐Cai Zhou
wiley   +1 more source

Formation of Molybdenum Deuteride at High Pressure: A Neutron Diffraction Study. [PDF]

open access: yesInorg Chem
Wei Z   +5 more
europepmc   +1 more source

Metabolically-incorporated deuterium in myelin localized by neutron diffraction and identified by mass spectrometry. [PDF]

open access: yesCurr Res Struct Biol, 2022
Baumann A   +4 more
europepmc   +1 more source

Rapid Mechanochemical Synthesis of Oxyhalide Superionic Conductor: Time‐Resolved Structural Evolution

open access: yesSmall Methods, EarlyView.
Time‐resolved synchrotron X‐ray scattering coupled with mechanochemical synthesis reveals the structural evolution of oxyhalide superionic conductors. Oxygen incorporation governs reaction kinetics, amorphization, and microstructural transformations, while enabling efficient Li‐ion diffusion. This study highlights critical correlations between reaction
Denys Butenko   +15 more
wiley   +1 more source

Crystal structure of diacetylene unveiled by X-ray and neutron diffraction, Raman spectroscopy and periodic DFT. [PDF]

open access: yesIUCrJ
Lopes Cavalcante L   +8 more
europepmc   +1 more source

Mapping the Residual Stress Distribution in Polycrystalline Quartz Tiger's Eye Using Raman Spectroscopy

open access: yesSmall Methods, EarlyView.
Residual stresses in Tiger’s Eye quartz have been mapped by combining Raman spectroscopy and electron back scatter diffraction. The study quantified stress distributions likely formed during cooling due to the anisotropy of thermal contraction. This non‐destructive methodology provides a reliable baseline for mapping stress in both natural polycrystals
Genevieve C. Kidman   +4 more
wiley   +1 more source

Recycling End‐of‐Life Solid Oxide Cell Interconnect Assemblies into Commercial‐Grade AISI 304 Stainless Steels

open access: yessteel research international, EarlyView.
This study validates a recycling pathway for converting interconnect assemblies from end‐of‐life SOC stacks into commercial‐grade AISI 304 steels. Using scrap‐based steelmaking operations, austenitic cast steels with <4.0% δ‐ferrite are successfully produced.
Jeraldine Lastam   +7 more
wiley   +1 more source

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