Results 11 to 20 of about 4,456 (184)

A comparison of the effectiveness of QuEChERS, FaPEx and a modified QuEChERS method on the determination of organochlorine pesticides in ginseng

open access: yesPLOS ONE, 2021
This study provides a review of methods used in the determination of organochlorine pesticides (OCPs) in ginseng and compares the effectiveness of three extraction methods (Quick, Easy, Cheap, Effective, Rugged, and Safe (QuEChERS), a modified QuEChERS and a Fast Pesticide Extraction (FaPEx)) in the analyses of 20 OCPs in ginseng root samples. For each
Pennante Bruce-Vanderpuije   +7 more
openaire   +5 more sources

QuEChERS as alternative extraction procedure in doping analyses

open access: yesDrug Testing and Analysis, 2023
AbstractQuEChERS is a dispersive solid phase extraction commonly applied in food analysis for residues, such as pesticides or mycotoxins for more than 20 years. Due to the quick and easy sample preparation procedure, a QuEChERS method based on ammonium acetate combined with formic acid in acetonitrile was tested for the preparation of urine samples for
Daniel Derwand   +4 more
openaire   +4 more sources

Extraction of ochratoxin A in bread samples by the QuEChERS methodology [PDF]

open access: yesFood Chemistry, 2012
A QuEChERS method for the extraction of ochratoxin A (OTA) from bread samples was evaluated. A factorial design (2(3)) was used to find the optimal QuEChERS parameters (extraction time, extraction solvent volume and sample mass). Extracts were analysed by LC with fluorescence detection.
Paíga, Paula   +7 more
openaire   +3 more sources

Determination of chloramphenicol residue in poultry eggs by QuEChERS combined with high performance liquid chromatography-tandem mass spectrometry

open access: yesZhongguo shipin weisheng zazhi, 2023
ObjectiveTo develop a method for determination of chloramphenicol residue in poultry eggs (hen egg, duck egg, quail egg, and goose egg) using QuEChERS (Quick, Easy, Cheap, Effective, Rugged, Safe) protocols combined with high performance liquid ...
ZHAO Sa   +7 more
doaj   +1 more source

Pesticide-Residue Analysis in Soils by the QuEChERS Method: A Review

open access: yesMolecules, 2022
Pesticides are among the most important contaminants worldwide due to their wide use, persistence, and toxicity. Their presence in soils is not only important from an environmental point of view, but also for food safety issues, since such residues can migrate from soils to food.
Miguel Ángel González-Curbelo   +2 more
openaire   +3 more sources

Development of QuEChERS/HPLC technique for the determination of veterinary drug residues in beef samples [PDF]

open access: yesSongklanakarin Journal of Science and Technology (SJST), 2023
The application of antibiotics in animals for therapeutic and growth promotion purposes and to meet the need to increase meat production has been reported to cause the development of antibiotic resistance and other health risks due to the consumption ...
Abibat Monisola Junaid   +9 more
doaj  

Determination of 12 Mycotoxins in Seasoning Flour Products by QuEChERS-SPE-Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry

open access: yesShipin gongye ke-ji, 2022
A method was developed for the residual quantity determination of 12 mycotoxins in seasoning flour products by QuEChERS-SPE-ultra performance liquid chromatography-tandem mass spectrometry. The samples were extracted with formic acid acetonitrile aqueous
Ziting XU   +6 more
doaj   +1 more source

Determination of 44 Organic Pollutants in Groundwater by Gas Chromatography-Triple Quadrupole Mass Spectrometry

open access: yesYankuang ceshi, 2021
BACKGROUND Organic pollutants such as organochlorine, polycyclic aromatic hydrocarbons and phthalate in groundwater are potential threats to the ecological environment and human health.
YU Lei, ZHANG Xiao-yi
doaj   +1 more source

Quechers approach to the Alternaria mycotoxins detection in wheat: The recovery study [PDF]

open access: yesZbornik Matice Srpske za Prirodne Nauke, 2022
The performance of the QuEChERS extraction followed by the LC-MS/ MS analytical method was evaluated in terms of Alternaria mycotoxins recovery from the wheat.
Bursić Vojislava P.   +8 more
doaj   +1 more source

QuEChERS extraction of benzodiazepines in biological matrices

open access: yesJournal of Pharmaceutical Analysis, 2013
Two common analytical chemical problems often encountered when using chromatographic techniques in drug analysis are matrix interferences and ion suppression. Common sample preparation often involves the dilution of the sample prior to injection onto an instrument, especially for liquid chromatography-mass spectrometry (LC-MS) analyses.
Jessica L. Westland, Frank L. Dorman
openaire   +3 more sources

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