Results 131 to 140 of about 17,786 (291)

Field‐Frustrated Cooperative Distortions: Suppressing Jahn‐Teller Ordering via Microwave Annealing

Advanced Science, EarlyView.
Microwave annealing decouples local Jahn‐Teller distortions from long‐range cooperative ordering in CuFe2O4, stabilizing a metastable cubic phase that remains locally distorted yet globally symmetry‐frustrated. Synchrotron XRD, PDF, XPS, and in situ thermal cycling reveal how non‐equilibrium MW‐phonon interactions suppress cooperative orbital‐lattice ...
Daryoosh Vashaee, Kelvin Dsouza
wiley   +1 more source

Taming Flexibility: Synergistic Pore and Polarity Engineering in a MOF for High‐Efficiency Xe/Kr Separation

Advanced Science, EarlyView.
Through a mixed‐ligand strategy that precisely regulates pore size and framework polarity, the Xe adsorption behavior is transformed from flexible to near‐rigid. ZIF‐7‐Cl(20) achieves sensitive recognition, efficient capture, and high selectivity for Xe, enabling high‐efficiency separation from Xe/Kr mixtures.
Tao Zhao, Xue Wang, Youjin Gong, Siqi Dong, Shunshun Xiong, Hui Xu, Aziz Bakhtiyarovich Ibragimov, Thamraa Alshahrani, He Zheng, Lin Li, Junkuo Gao   +10 more
wiley   +1 more source

Synchrotron powder diffraction Rietveld refinement of MgB20 crystal structure

, 2002
The crystal structure of MgB20 has been investigated by X-ray and synchrotron powder diffraction at room temperature. As it happens in other metal-boron systems, the Rietveld refinement of this magnesium boron-rich phase shows a structure derived ...
P. Manfrinetti, S. Brutti, M. Colapietro, L. Barba, COLAPIETRO, Marcello, BRUTTI, SERGIO, BALDUCCI, Giovanni, A. Palenzona, G. Balducci   +8 more
core   +1 more source

3D‐Mixer‐Assisted High‐Entropy Doping of LiNiO2 for Co‐Free Ni‐Rich Cathodes in Lithium‐Ion Batteries

Advanced Science, EarlyView.
High‐entropy doping of Co‐free Ni‐rich LiNiO2 cathodes is achieved through a scalable 3D mixing process. Multi‐element incorporation stabilizes the layered structure, alleviates Li/Ni disorder and electrode swelling, and enhances cycling stability. This approach underscores the potential of high‐entropy strategies to deliver structurally robust and ...
Seung Ri Kim, Thillai Govindaraja Senthamaraikannan, Jun Jae Myeong, Hyung Do Kim, Dong‐Hee Lim, Eun Mi Kim, Sang Mun Jeong   +6 more
wiley   +1 more source

Utilization of marine snails for the sustainable synthesis and crystallographic characterization of nano-crystallite hydroxyapatite

Hybrid Advances
In the present investigation, several biogenic sources of calcium were used to produce HAp nanomaterials by the use of a typical wet chemical precipitation technique. To determine the development of HAp nanocrystals, a variety of characterization methods
Md. Kawcher Alam, Md. Sahadat Hossain, Md. Anayet Ullah, Newaz Mohammed Bahadur, Samina Ahmed   +4 more
doaj   +1 more source

Atomically Modulating Competing Exchange Interactions in Centrosymmetric Skyrmion Hosts GdRu2X2 (X = Si and Ge)

Advanced Electronic Materials, EarlyView.
Our work bridges the gap between skyrmion discovery and material design by demonstrating how atomic‐scale control of exchange interactions enables tunable skyrmion phase transitions in centrosymmetric magnetic metals. ABSTRACT Magnetic skyrmions are topologically protected spin states that hold promise for shaping the future of electronics.
Dasuni N. Rathnaweera, Xudong Huai, K. Ramesh Kumar, Michał J. Winiarski, Tomasz Klimczuk, Allana G. Iwanicki, Satya K. Kushwaha, Martin Mourigal, Tyrel M. McQueen, Thao T. Tran   +9 more
wiley   +1 more source

COMPOUND REFINEMENT RIETVELD SUPERCONDUCTING YBa2Cu3O7

Revista Peruana de Química e Ingeniería Química, 2006
The superconductor YBa2Cu3O7 compound was synthesized by the sol-gel technique. The pattern of X-ray diffraction showed that the ceramic oxide crystallized in an orthorhombic structure. The structure analysis was performed by allowing Rietveld refinement obtain network parameters, the atomic positions, occupancy of atomic sites, identify dollies and ...
González, J.C., Osorio, Ana, Bustamante, Ángel, Carhuancho, Maria, Castro, Amado, Marín, Rómulo   +5 more
openaire   +1 more source

X-ray diffraction and Rietveld structural refinement of selected fluoroperovskites [PDF]

, 2000
This study presents an X-ray diffraction analysis and Rietveld structural refinement of selected synthetic fluoroperovskite-type compounds including the Na1-xKxMgF3 solid solution series in addition to synthetic analogues of cryolite (Na2NaAlF6) and ...
Ross, Kirk Campbell
core  

Averaging the intensity of many-layered structures for accurate stacking-fault analysis using Rietveld refinement

, 2016
Many technologically important synthetic and natural materials display stacking faults which lead to complex peak broadenings, asymmetries and shifts in their powder diffraction patterns.
Evans, J.S.O., Lewis, J.W., Coelho, A.A.
core   +1 more source

Degradation Mechanism of Phosphate‐Based Li‐NASICON Conductors in Alkaline Environment

Advanced Energy Materials, Volume 15, Issue 11, March 18, 2025.
The presence of water in the cathode of a Li‐air battery shifts reactions to produce LiOH, creating a corrosive, alkaline environment. This study investigates the alkaline stability of the common Li‐NASICON solid‐state conductor chemistries through a systematic experimental study combined with computational modeling to understand the degradation ...
Benjamin X. Lam, Zhuohan Li, Tara P. Mishra, Gerbrand Ceder   +3 more
wiley   +1 more source