Crystal structure of polymeric triphenyltin triflate
The crystal structure of the previously known title compound, Ph3SnO3SCF3, was determined by single-crystal X-ray diffraction; it comprises a one-dimensional polymeric structure and pentacoordinated Sn atoms.
Beckmann Jens, Lork Enno, Mallow Ole
doaj +1 more source
Synthesis and Characterization of platinum – selenium Derivatives: X-ray Structure of \u3cem\u3etrans\u3c/em\u3e-Pt(Pet\u3csub\u3e3\u3c/sub\u3e)\u3csub\u3e2\u3c/sub\u3e(SePh)\u3csub\u3e2\u3c/sub\u3e [PDF]
The crystal structure of trans-[((bis)triethylphosphine)(bis(phenylselenato))platinum (II)] has been determined by single crystal X-ray diffraction. Crystallization occurs in the triclinic space group P-1 (No. 2) with a = 8.9964(2) Å, b = 11.5103(2) Å, c
Lindeman, Sergey V., Rudd, Martin D.
core +1 more source
Ground State of Relaxor Ferroelectric $Pb(Zn_{1/3}Nb_{2/3})O_3$
High energy x-ray diffraction measurements on Pb(Zn$_{1/3}$Nb$_{2/3}$)O$_3$ (PZN) single crystals show that the system does not have a rhombohedral symmetry at room temperature as previously believed.
A. Lebon +28 more
core +1 more source
Multimodal Data‐Driven Microstructure Characterization
A self‐consistent autonomous workflow for EBSP‐based microstructure segmentation by integrating PCA, GMM clustering, and cNMF with information‐theoretic parameter selection, requiring no user input. An optimal ROI size related to characteristic grain size is identified.
Qi Zhang +4 more
wiley +1 more source
A number of salophen ligands and their Zn, Ni, and Pd complexes were synthesized by an efficient one-pot mechanosynthesis protocol. The reaction products were characterized by means of complementary solid-state techniques, i.e., powder X-ray diffraction,
Luca Leoni +7 more
doaj +1 more source
Microstructure Design of Steel‐Spinel Composites via Spark Plasma Sintering Process
This study illustrates how spark plasma sintering at reduced oxygen partial pressure enables controlled formation of steel‐spinel composites through tailored redox reactions and cation exchange. Comparison of the MgO–Fe2O3, steel–(MgO+Cr2O3), and steel–(MgO+Fe2O3) systems shows how oxygen activity and interface chemistry govern spinel formation, phase ...
Mahnaz Mehdizadehlima +4 more
wiley +1 more source
Absence of anomalous negative lattice-expansion for polycrystalline sample of Tb2Ti2O7
High resolution X-ray powder-diffraction experiments on a well-characterized polycrystalline sample of the spin liquid Tb2Ti2O7 reveal that it shows normal positive thermal-expansion above 4 K, which does not agree with the intriguing anomalous negative ...
Anderson P. W. +20 more
core +1 more source
Tailoring Functional Properties of Ti–Ni–Cu Shape Memory Alloy Thin Films for MEMS Actuators
A comprehensive study of critical parameters required to develop well‐performing Ti–Ni–Cu thin film shape memory alloy microactuators is provided. Materials science and device integration aspects are integrated by addressing structural and physical relationships using complementary characterization techniques as well as a practical fabrication solution
Elaheh Akbarnejad +6 more
wiley +1 more source
Superconducting and ferromagnetic phases induced by lattice distortions in SrFe2As2
Single crystals of SrFe2As2 grown using a self-flux solution method were characterized via x-ray, transport and magnetization studies, revealing a superconducting phase below T_c = 21 K characterized by a full electrical resistivity transition and ...
Johnpierre Paglione +4 more
core +1 more source
Production of MgO/TiC Composites From MgO‐C Recyclates Using Spark Plasma Sintering
Using the spark plasma sintering technique, MgO/TiC composites are manufactured from recycled MgO‐C refractories stemming from the steel production that were mixed with titanium powder. This article shows, how the size of the Ti grains and their distribution in the powder mixture affect the local carbon concentration in TiC.
Jiayan Yu +3 more
wiley +1 more source

