Solid-state NMR characterisation of the thermal transformation of a Hungarian white illite [PDF]
1H, 27Al, 29Si and 39K solid-state NMR are reported from a Hungarian illite 2:1 clay for samples heated up 1600 °C. This single-phase sample has a small amount of aluminium substitution in the silica layer and very low iron-content (0.4 wt%).
Carroll, Donna L. +3 more
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Effects of radial radio-frequency field inhomogeneity on MAS solid-state NMR experiments [PDF]
Radio-frequency field inhomogeneity is one of the most common imperfections in NMR experiments. They can lead to imperfect flip angles of applied radio-frequency (rf) pulses or to a mismatch of resonance conditions, resulting in artefacts or degraded ...
K. Aebischer, Z. Tošner, M. Ernst
doaj +1 more source
Acidity and Basicity of Solid Acid Catalysts Studied by Solid-State NMR
Solid-state nuclear magnetic resonance (NMR) is an important technique to study the acidity and basicity of solid catalysts. Here we review some research works carried out in our laboratory, including studies on the acidity of metal oxides under ...
Xin CHEN +3 more
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Ultra-high resolution 17O solid-state NMR spectroscopy of biomolecules : a comprehensive spectral analysis of monosodium L-glutamate·monohydrate [PDF]
Monosodium L-glutamate monohydrate, a multiple oxygen site (eight) compound, is used to demonstrate that a combination of high-resolution solid-state NMR spectroscopic techniques opens up new possibilities for (17)O as a nuclear probe of biomolecules ...
Howes, Andy P. +29 more
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ssNMRlib: a comprehensive library and tool box for acquisition of solid-state nuclear magnetic resonance experiments on Bruker spectrometers [PDF]
We introduce ssNMRlib, a comprehensive suite of pulse sequences and jython scripts for user-friendly solid-state nuclear magnetic resonance (NMR) data acquisition, parameter optimization and storage on Bruker spectrometers.
A. Vallet +3 more
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Solid-State NMR Study of New Copolymers as Solid Polymer Electrolytes
We report the analysis of comb-like polymers by solid-state NMR. The polymers were previously evaluated as solid-polymer-electrolytes (SPE) for lithium-polymer-metal batteries that have suitable ionic conductivity at 60 °C.
Jean-Christophe Daigle +3 more
doaj +1 more source
Solid-state NMR has proven to be a versatile technique for studying the chemical structure, 3D structure and dynamics of all sorts of chemical compounds.
Mustapha El Hariri El Nokab +1 more
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Structural study of La1-xYxScO3, combining neutron diffraction, solid-state NMR, and first-principles DFT calculations [PDF]
The solid solution La1-xYxScO3 (x = 0, 0.2, 0.4, 0.6, 0.8, and 1) has been successfully synthesized using conventional solid-state techniques. Detailed structural characterization has been undertaken using high-resolution neutron powder diffraction and ...
Johnston KE +12 more
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Biological Solid-state NMR at ETH Zurich
Solid-state Magnetic Resonance has been greatly developed over the past decade. Higher field spectrometers and other technical developments are expected to lead to further significant improvements.
Giorgia Zandomeneghi +2 more
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Asymmetrically Substituted Phospholes as Ligands for Coinage Metal Complexes
A series of coinage metal complexes asymmetrically substituted 2,5-diaryl phosphole ligands is reported. Structure, identity, and purity of all obtained complexes were corroborated with state-of-the-art techniques (multinuclear NMR, mass spectrometry ...
Fabian Roesler +2 more
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